1,4-Piperazinedicarboxylic acid, 2-[[(1,1-dimethylethyl)amino]carbonyl]-, 4-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Base Information

Chemical Name:1,4-Piperazinedicarboxylic acid, 2-[[(1,1-dimethylethyl)amino]carbonyl]-, 4-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-
CAS No.:150323-34-5
Molecular Formula:C22H33N3O5
Molecular Weight:419.521
Hs Code.:
Mol file:150323-34-5.mol

Synonyms:

Suppliers and Price of 1,4-Piperazinedicarboxylic acid, 2-[[(1,1-dimethylethyl)amino]carbonyl]-, 4-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Piperazinedicarboxylic acid, 2-[[(1,1-dimethylethyl)amino]carbonyl]-, 4-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Piperazinedicarboxylic acid, 2-[[(1,1-dimethylethyl)amino]carbonyl]-, 4-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

There total 7 articles about 1,4-Piperazinedicarboxylic acid, 2-[[(1,1-dimethylethyl)amino]carbonyl]-, 4-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 171504-92-0
5-tert-Butylcarbamoyl-2,3-dihydro-pyrazine-1,4-dicarboxylic acid 4-benzyl ester 1-tert-butyl ester

: 150323-34-5
N-tert-butyl-4-<(1,1-dimethylethoxy)carbonyl>-1-<(phenylmethyl)carbonyl>piperazine-2(S)-carboxamide

Guidance literature:: With hydrogen; <(R)-BINAP(COD)Rh>OTf; In methanol; at 40 ℃; for 18h; under 52504.2 Torr;
DOI:10.1016/0040-4039(95)01345-I

Reference yield: 92.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 150323-35-6,171866-36-7,128019-61-4
t-butyl (S)-3-(tert-butylcarbamoyl)-piperazine-1-carboxylate

: 150323-34-5
N-tert-butyl-4-<(1,1-dimethylethoxy)carbonyl>-1-<(phenylmethyl)carbonyl>piperazine-2(S)-carboxamide

Guidance literature:: DOI:10.1021/jm980053f

Reference yield: 85.0%

: 75-64-9
tert-butylamine

: 150407-69-5
[2S]-1-benzyloxycarbonyl-4-t-butoxycarbonylpiperazine-2-carboxylic acid

: 150323-34-5
N-tert-butyl-4-<(1,1-dimethylethoxy)carbonyl>-1-<(phenylmethyl)carbonyl>piperazine-2(S)-carboxamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; for 18h;
DOI:10.1021/jm00047a001