4-Phenyl-2H-1,3-dithiole

Base Information

Chemical Name:4-Phenyl-2H-1,3-dithiole
CAS No.:15112-40-0
Molecular Formula:C9H8S2
Molecular Weight:180.295
Hs Code.:
DSSTox Substance ID:DTXSID90504486
Nikkaji Number:J2.300.636G
Wikidata:Q82359023
Mol file:15112-40-0.mol

Synonyms:4-phenyl-1,3-dithiole;4-Phenyl-2H-1,3-dithiole;15112-40-0;SCHEMBL1577299;DTXSID90504486

Suppliers and Price of 4-Phenyl-2H-1,3-dithiole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Phenyl-2H-1,3-dithiole

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:180.00674260
Heavy Atom Count:11
Complexity:157

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1SC=C(S1)C2=CC=CC=C2

Technology Process of 4-Phenyl-2H-1,3-dithiole

There total 4 articles about 4-Phenyl-2H-1,3-dithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 77633-43-3
Chloromethylsulfanylethynyl-benzene

: 15112-40-0
4-phenyl-1,3-dithiole

Guidance literature:: With sodium sulfide; In methanol; N,N-dimethyl-formamide; for 9h;

Reference yield: 58.0%

: 4217-54-3
9,10-dihydro-10-methylacridine

: 4-phenyl-1,3-dithiolium perchlorate

: 15112-40-0
4-phenyl-1,3-dithiole

: 26456-05-3
10-methylacridinium perchlorate

Guidance literature:: In tetrahydrofuran; at 80 ℃;
DOI:10.1007/s10593-006-0272-2

Reference yield:

: 536-74-3
phenylacetylene

: 15112-40-0
4-phenyl-1,3-dithiole

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / butyllithium / hexane; diethyl ether / 0.33 h

2: 85 percent / Na₂S / methanol; dimethylformamide / 9 h

With sodium sulfide; n-butyllithium; In methanol; diethyl ether; hexane; N,N-dimethyl-formamide;