2,2-Dimethyl-4-oxohexanoic acid

Base Information

Chemical Name:2,2-Dimethyl-4-oxohexanoic acid
CAS No.:15118-53-3
Molecular Formula:C8H14O3
Molecular Weight:158.197
Hs Code.:
Mol file:15118-53-3.mol

Synonyms:2,2-Dimethyl-4-oxo-hexanoic acid;2,2-Dimethyl-4-oxo-hexansaeure;

Suppliers and Price of 2,2-Dimethyl-4-oxohexanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,2-Dimethyl-4-oxohexanoic acid

Chemical Property:

Melting Point:87-88℃
Boiling Point:268℃
Flash Point:130℃
PSA：54.37000
Density:1.038
LogP:1.46640

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2-Dimethyl-4-oxohexanoic acid

There total 5 articles about 2,2-Dimethyl-4-oxohexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17347-61-4
2,2-dimethylsuccinic anhydride

: 557-20-0
diethylzinc

: 3,3-dimethyl-4-oxo-hexanoic acid

: 15118-53-3
2,2-dimethyl-4-oxohexanoic acid

Guidance literature:: With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; para-fluorostyrene; In tetrahydrofuran; at 0 ℃; for 4h; Title compound not separated from byproducts;
DOI:10.1021/ja044588b

Reference yield:

: 597-43-3
2,2-dimethylsuccinic acid

: 15118-53-3
2,2-dimethyl-4-oxohexanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic anhydride / CH₂Cl₂ / 1 h / 0 °C

2: Ni(COD)2; 2,2'-bipyridyl; 4-fluorostyrene / tetrahydrofuran / 4 h / 0 °C

With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; para-fluorostyrene; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja044588b

Reference yield:

: 54491-23-5
2,2-dimethyl-4-hydroxyhexanoic acid γ-lactone

: 15118-53-3
2,2-dimethyl-4-oxohexanoic acid

Guidance literature:: With sodium hydroxide; sodium hypochlorite; ruthenium(IV) oxide; Yield given. Multistep reaction; 1.) water, 1 h, ambient temperature, 2.) below 10 deg C;
DOI:10.1021/jo00296a063