Technology Process of 2-Butenoic acid, 3-[3-(trimethylsilyl)phenyl]-, ethyl ester, (E)-
There total 5 articles about 2-Butenoic acid, 3-[3-(trimethylsilyl)phenyl]-, ethyl ester, (E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) Mg, I2 / 1.) anhydrous THF, 4 h, 60 deg C, 2.) THF
2: 97 percent / H2O, 10percent HCl / methanol / 1 h / Ambient temperature
3: 1.) t-BuOK / 1.) anhydrous THF, 30 min, RT, 2.) THF, RT, 24 h
With
hydrogenchloride; potassium tert-butylate; water; iodine; magnesium;
In
methanol;
DOI:10.1016/0040-4020(95)00805-I
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / TsOH / benzene / 20 h / Heating
2: 1.) Mg, I2 / 1.) anhydrous THF, 4 h, 60 deg C, 2.) THF
3: 97 percent / H2O, 10percent HCl / methanol / 1 h / Ambient temperature
4: 1.) t-BuOK / 1.) anhydrous THF, 30 min, RT, 2.) THF, RT, 24 h
With
hydrogenchloride; potassium tert-butylate; water; iodine; toluene-4-sulfonic acid; magnesium;
In
methanol; benzene;
DOI:10.1016/0040-4020(95)00805-I
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / H2O, 10percent HCl / methanol / 1 h / Ambient temperature
2: 1.) t-BuOK / 1.) anhydrous THF, 30 min, RT, 2.) THF, RT, 24 h
With
hydrogenchloride; potassium tert-butylate; water;
In
methanol;
DOI:10.1016/0040-4020(95)00805-I
![2-(3-bromophenyl)-2-methyl-[1,3]dioxolane](/Databaselist/images/loading.webp)
