Technology Process of Benzenamine, 5-bromo-2-chloro-, hydrochloride
There total 1 articles about Benzenamine, 5-bromo-2-chloro-, hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-bromo-1-chloro-2-nitrobenzene;
With
hydrogen;
nickel;
In
ethyl acetate;
for 5h;
under 2844.39 Torr;
With
hydrogenchloride;
In
diethyl ether; ethyl acetate;
for 1h;
- Guidance literature:
-
5-bromo-2-chloroaniline hydrochloride;
With
hydrogenchloride;
In
water; acetonitrile;
at 5 ℃;
for 0.166667h;
With
sodium nitrite;
In
water; acetonitrile;
at -5 ℃;
for 0.25 - 0.333333h;
With
sulfur dioxide; copper dichloride;
In
water; acetic acid; acetonitrile;
at 0 - 20 ℃;
for 1.5h;
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 ℃;