Bicyclo[2.2.1]hept-2-ene,5-methoxy-exo-

Base Information

• Chemical Name: Bicyclo[2.2.1]hept-2-ene,5-methoxy-exo-
• CAS No.: 17190-87-3
• Molecular Formula: C₈H₁₂O
• Molecular Weight: 124.183
• Mol file: 17190-87-3.mol

Synonyms:2-Norbornene,5-methoxy-, exo- (8CI); Bicyclo[2.2.1]hept-2-ene, 5-methoxy-, exo-;2-exo-Methoxy-5-norbornene; 5-exo-Methoxynorbornene;exo-5-Methoxybicyclo[2.2.1]hept-2-ene

Chemical Property of Bicyclo[2.2.1]hept-2-ene,5-methoxy-exo-

Chemical Property:

• Vapor Pressure: 4.53mmHg at 25°C
• Boiling Point: 152.1°C at 760 mmHg
• Flash Point: 36.3°C
• PSA: 9.23000
• Density: 0.99g/cm³
• LogP: 1.59740

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]hept-2-ene,5-methoxy-exo-

There total 3 articles about Bicyclo[2.2.1]hept-2-ene,5-methoxy-exo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + C14H15N2O2S(1-)*Na(1+) → 5-exo-methoxybicyclo[2.2.1]hept-2-ene (17190-87-3,17190-92-0,56663-04-8) + bicyclo[2.2.1]hepta-2,5-diene (121-46-0) + (3R,4S,6S)-3-Methoxy-tricyclo[2.2.1.02,6]heptane + 4-Methoxy-bicyclo[3.1.1]hept-2-ene

Guidance literature:

With sodium methylate; at 20 ℃; Product distribution; Mechanism; Irradiation;

DOI:10.1039/c39940001065

Reference yield:

methanol (67-56-1) + spiro(bisyclo<2.2.1>hept-5-ene-2,3'-diazirine) → 5-exo-methoxybicyclo[2.2.1]hept-2-ene (17190-87-3,17190-92-0,56663-04-8) + bicyclo[2.2.1]hepta-2,5-diene (121-46-0) + (3R,4S,6S)-3-Methoxy-tricyclo[2.2.1.02,6]heptane + 4-Methoxy-bicyclo[3.1.1]hept-2-ene

Guidance literature:

at 20 ℃; Product distribution; Mechanism; Irradiation; var. additive reagents;

DOI:10.1039/c39940001065

Reference yield:

methanol (67-56-1) + quadricyclo[2.2.1.0.0]heptane (278-06-8) → 3-methoxynortricyclene (21516-65-4) + 5-exo-methoxybicyclo[2.2.1]hept-2-ene (17190-87-3,17190-92-0,56663-04-8) + (1S,4R)-7-Methoxy-bicyclo[2.2.1]hept-2-ene + 1-Cyanonaphthalene (86-53-3)

Guidance literature:

With 1-Cyanonaphthalene; Product distribution; Irradiation;

DOI:10.1002/(SICI)1099-1395(199802)11:2<101::AID-POC978>3.0.CO;2-G

upstream raw materials:

methanol

quadricyclo[2.2.1.0.0]heptane

Downstream raw materials:

p-Toluolsulfonsaeure-<6endo-methoxy-2endo-norbornyl>ester

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