2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine

Base Information

Chemical Name:2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine
CAS No.:154403-27-7
Molecular Formula:C₁₈H₂₁N₉
Molecular Weight:363.425
Hs Code.:
Mol file:154403-27-7.mol

Synonyms:tris(3,5-dimethylpyrazolyl-1-yl)-1,3,5-triazine;2,4,6-tri(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine;2,4,6-tris(3,5-dimethyl-1H-pyrazol-1-yl)-1,3,5-triazine;tris(3,5-dimethylpyrazol-1-yl)-s-triazine;2,4,6-tris(3,5-dimethyl-pyrazol-1-yl)-1,3,5-triazine;

Suppliers and Price of 2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 11 raw suppliers

Chemical Property of 2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine

Chemical Property:

PSA：92.13000
LogP:2.27910

Purity/Quality:: ≥99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine

There total 1 articles about 2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.7%

: 67-51-6
3,5-dimethyl-1H-pyrazole

: 108-77-0
1,3,5-trichloro-2,4,6-triazine

: 154403-27-7
2,4,6-tris(3,5-dimethyl-pyrazol-1-yl)-1,3,5-triazine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 23h; Inert atmosphere; Reflux;
DOI:10.1021/ja411067a

Reference yield: 65.0%

: 105286-78-0
bis(pentafluorophenyl)(1,5-cyclo-octadiene)palladium(II)

: 154403-27-7
2,4,6-tris(3,5-dimethyl-pyrazol-1-yl)-1,3,5-triazine

: 501035-45-6
[Pd(C₆F₅)2(2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine)]

Guidance literature:: In tetrahydrofuran; under N2 atm. to soln. Me2-TpzT in THF was added Pd(C6F5)2(cod) and stirred for 2 h at room temp.; soln. was concd., hexane was added, ppt. was filtered and washed with hexane; elem. anal.;
DOI:10.1021/ic020522a

Reference yield: 57.0%

: 110-54-3
hexane

: 501035-47-8
Pd(m-C₆ClF₄)2(1,5-cyclooctadiene)

: 154403-27-7
2,4,6-tris(3,5-dimethyl-pyrazol-1-yl)-1,3,5-triazine

: [Pd(m-C₆ClF₄)2(2,4,6-tris(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine)]*1/4C₆H₁₄

Guidance literature:: In acetone; under N2 atm. to soln. Me2-TpzT in acetone was added Pd(C6ClF4)2(cod) and stirred for 2 h; soln. was evapd. to dryness, residue was washed with pentane and recrystd. from CH2Cl2/hexane; elem. anal.;
DOI:10.1021/ic020522a