2-Propenoic acid, 3-[(2S)-3,4-dihydro-2H-pyran-2-yl]-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-

Base Information

Chemical Name:2-Propenoic acid, 3-[(2S)-3,4-dihydro-2H-pyran-2-yl]-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-
CAS No.:155897-15-7
Molecular Formula:C24H32O3
Molecular Weight:368.516
Hs Code.:
Mol file:155897-15-7.mol

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Chemical Property of 2-Propenoic acid, 3-[(2S)-3,4-dihydro-2H-pyran-2-yl]-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-

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Technology Process of 2-Propenoic acid, 3-[(2S)-3,4-dihydro-2H-pyran-2-yl]-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)-

There total 6 articles about 2-Propenoic acid, 3-[(2S)-3,4-dihydro-2H-pyran-2-yl]-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (2Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 100-73-2
acrolein dimer

: 155795-46-3
[bis(2,2,2-trifluoroethoxy)phosphoryl]acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester

: 155897-15-7
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2Z)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

: 155897-13-5
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2E)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

: 155795-47-4
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2E)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

Guidance literature:: With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/ol991387h

Reference yield: 12.0%

: 100-73-2
acrolein dimer

: (Bis-p-tolyloxy-phosphoryl)-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 155897-15-7
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2Z)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

: 155897-14-6
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2Z)-3-[(2S)-3,4-dihydro-2H-pyran-2-yl]acrylate

: 155795-47-4
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2E)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

Guidance literature:: With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; Title compound not separated from byproducts;
DOI:10.1021/ol991387h

Reference yield:

: 100-73-2
acrolein dimer

: 155795-46-3
[bis(2,2,2-trifluoroethoxy)phosphoryl]acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester

: 155897-15-7
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2Z)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

: 155897-13-5
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2E)-3-[(2R)-3,4-dihydro-2H-pyran-2-yl]acrylate

: 155897-14-6
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl (2Z)-3-[(2S)-3,4-dihydro-2H-pyran-2-yl]acrylate

Guidance literature:: With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 7h;
DOI:10.1021/ol0479242