bis(phenylethynyl)ytterbium(tetrahydrofuran)4

Base Information

Chemical Name:bis(phenylethynyl)ytterbium(tetrahydrofuran)4
CAS No.:723502-34-9
Molecular Formula:C₃₂H₄₂O₄Yb
Molecular Weight:663.723
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(phenylethynyl)ytterbium(tetrahydrofuran)4

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Technology Process of bis(phenylethynyl)ytterbium(tetrahydrofuran)4

There total 1 articles about bis(phenylethynyl)ytterbium(tetrahydrofuran)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: ytterbium(II) iodide

: 1004-22-4
phenylethynylsodium

: 723502-34-9
bis(phenylethynyl)ytterbium(tetrahydrofuran)4

Guidance literature:: In tetrahydrofuran; by a react. of YbI2 with phenylethynylsodium in THF;
DOI:10.1023/B:RUGC.0000007638.44196.89

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 723502-34-9
bis(phenylethynyl)ytterbium(tetrahydrofuran)4

: 145447-65-0
YbCl₂(tetrahydrofuran)2

: 723502-56-5
phenylethynylytterbium(II) chloride tetrahydrofuranate

Guidance literature:: In tetrahydrofuran; byproducts: Me3SiCCPh; Me3SiCl was added to a soln. of Yb-contg. compd. in THF (molar ratio 2:1); the mixt. was allowed to stand for a day at room temp.; the yellow solid was vac.-dried for 1 h at room temp.; the react. was carried out in evacuated sealed ampules; the solvent was vac. evapd., and the residue was treated with hexane; elem. anal.;
DOI:10.1023/B:RUGC.0000007638.44196.89