Tributyl(Methoxy)Silane

Base Information

• Chemical Name: Tributyl(Methoxy)Silane
• CAS No.: 15811-64-0
• Molecular Formula: C13H30OSi
• Molecular Weight: 230.466
• Mol file: 15811-64-0.mol

Synonyms:Tributyl-methoxy-silan;Silane,tributylmethoxy;Tributylmethoxysilane;tri-n-butylmethoxysilane;Methoxy-tri-n-butyl-silan;Methyl tributylsilyl ether;methoxytributyl silane;

Chemical Property of Tributyl(Methoxy)Silane

Chemical Property:

• Refractive Index: 1.4329
• Boiling Point: 239°C
• Flash Point: >110°C (>230°F)
• PSA: 9.23000
• LogP: 4.97860

Purity/Quality:

95.00% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tributyl(Methoxy)Silane

There total 7 articles about Tributyl(Methoxy)Silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

methanol (67-56-1) + tributyl(phenyl)silane (18510-29-7) → Tributylmethoxysilane (15811-64-0)

Guidance literature:

tributyl(phenyl)silane; With ammonia; iron(III) chloride; sodium amide; at 20 ℃; for 0.166667h;

methanol; With acetyl chloride; at 20 ℃; for 1h;

Reference yield:

methanol (67-56-1) + tributylsilane (998-41-4) → Tributylmethoxysilane (15811-64-0)

Guidance literature:

With sodium methylate;

DOI:10.1016/S0022-328X(00)86243-9

Reference yield:

tributylchlorosilane (995-45-9) → Tributylmethoxysilane (15811-64-0)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N

2: (i) tBuMgCl, Et₂O, (ii) (heating)

3: NaOMe

With sodium methylate; triethylamine;

DOI:10.1016/S0022-328X(00)86243-9

upstream raw materials:

n-butyl magnesium bromide

tetramethylorthosilicate

methanol

tributylsilane

Downstream raw materials:

tributylchlorosilane

tetrabutylsilane

hexabutyldisiloxane

tributylsilyl methacrylate

Refernces

• 1、 -. "METHOD FOR PRODUCING HYDROCARBON OXYSILICON COMPOUNDS". Page/Page column 6. . Retrieved 2012/01/15.
• 2、 Sun, Guang-Ri,He, Jin-Bao,Zhu, Hua-Jie,Pittman Jr., Charles U.. "Cleavage of arylalkylsilanes by sodium amide in liquid ammonia". . p. 619 - 622. Retrieved 2007/10/03.