1,10-BIS(MALEIMIDE)DECANE

Base Information

• Chemical Name: 1,10-BIS(MALEIMIDE)DECANE
• CAS No.: 39763-02-5
• Molecular Formula: C₁₈H₂₄N₂O₄
• Molecular Weight: 332.4
• Mol file: 39763-02-5.mol

Synonyms:1,10-Bis(maleimido)decane;1,10-Di(maleimido)decane; Bis(maleimido)decamethylene;Decamethylenedimaleimide; N,N'-Bismaleimido-1,10-decane;N,N'-Decamethylenebis[maleimide]; NSC 44753

Chemical Property of 1,10-BIS(MALEIMIDE)DECANE

Chemical Property:

• Boiling Point: 492.2oC at 760 mmHg
• Flash Point: 213.1oC
• PSA: 74.76000
• Density: 1.196g/cm3
• LogP: 1.83300

Purity/Quality:

99% ^*data from raw suppliers

1,10-BIS(MALEIMIDE)DECANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,10-BIS(MALEIMIDE)DECANE

There total 4 articles about 1,10-BIS(MALEIMIDE)DECANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C26H32N2O6 (1449656-08-9) → N,N'-Decamethylendimaleinimid (39763-02-5)

Guidance literature:

In 1,1,2,2-tetrachloroethane; at 120 ℃; for 12h;

DOI:10.1016/j.tetlet.2013.07.002

Reference yield: 90.0%

N-methoxycarbonylmaleimide (55750-48-6) + diaminodecane (646-25-3) → N,N'-Decamethylendimaleinimid (39763-02-5)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; for 3h; Ambient temperature;

DOI:10.1021/jm00087a010

Reference yield:

1,10-dibromodecane (4101-68-2) → N,N'-Decamethylendimaleinimid (39763-02-5)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 50 °C / Inert atmosphere

2: 1,1,2,2-tetrachloroethane / 12 h / 120 °C

With potassium carbonate; In N,N-dimethyl-formamide; 1,1,2,2-tetrachloroethane;

DOI:10.1016/j.tetlet.2013.07.002

upstream raw materials:

N-methoxycarbonylmaleimide

diaminodecane

1,10-dibromodecane

C₂₆H₃₂N₂O₆