(CO)3(1,2-bis(diphenylphosphino)ethane)MnF

Base Information

Chemical Name:(CO)3(1,2-bis(diphenylphosphino)ethane)MnF
CAS No.:364046-03-7
Molecular Formula:C₂₉H₂₄FMnO₃P₂
Molecular Weight:556.392
Hs Code.:

Synonyms:

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Chemical Property of (CO)3(1,2-bis(diphenylphosphino)ethane)MnF

Chemical Property:

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Technology Process of (CO)3(1,2-bis(diphenylphosphino)ethane)MnF

There total 4 articles about (CO)3(1,2-bis(diphenylphosphino)ethane)MnF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tetraethylammonium fluoride hydrate

: 247939-31-7
[fac-Mn(CO)3(1,2-bis(diphenylphosphino)ethane)(OH₂)]BF₄

: 364046-03-7
(CO)3(1,2-bis(diphenylphosphino)ethane)MnF

Guidance literature:: In dichloromethane; (Ar); stirred for 25 min; washed (H2O), CH2Cl2 removed (vac.), the residue dissolved in C6H6, filtered, evapd. (vac.);
DOI:10.1016/S0022-328X(01)00829-4

Reference yield:

: tetraethylammonium fluoride hydrate

: [(CO)3(1,2-bis(diphenylphosphino)ethane)Mn(OH₂)...FMn(1,2-bis(diphenylphosphino)ethane)(CO)3]BF₄

: 364046-03-7
(CO)3(1,2-bis(diphenylphosphino)ethane)MnF

Guidance literature:: In dichloromethane; (Ar); stirred for 3 h; the CH2Cl2 soln. sepd., washed (H2O), concd., hexane added, pptd. on cooling, collected;
DOI:10.1016/S0022-328X(01)00829-4

Reference yield:

: 247939-31-7
[fac-Mn(CO)3(1,2-bis(diphenylphosphino)ethane)(OH₂)]BF₄

: 7681-49-4
sodium fluoride

: 364046-03-7
(CO)3(1,2-bis(diphenylphosphino)ethane)MnF

: [(CO)3(1,2-bis(diphenylphosphino)ethane)Mn(OH₂)...FMn(1,2-bis(diphenylphosphino)ethane)(CO)3]BF₄

Guidance literature:: In dichloromethane; water; (Ar); excess NaF/H2O added to complex/CH2Cl2, stirred for 2.5 h; the CH2Cl2 soln. sepd., washed (H2O), concd., hexane added, crystd. on cooling; elem. anal.;
DOI:10.1016/S0022-328X(01)00829-4