(CO)3(1,2-bis(diphenylphosphino)ethane)MnCl

Base Information Edit

Chemical Name:(CO)3(1,2-bis(diphenylphosphino)ethane)MnCl
CAS No.:49695-20-7
Molecular Formula:C₂₉H₂₄ClMnO₃P₂
Molecular Weight:572.846
Hs Code.:
Mol file:49695-20-7.mol

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Chemical Property of (CO)3(1,2-bis(diphenylphosphino)ethane)MnCl Edit

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Technology Process of (CO)3(1,2-bis(diphenylphosphino)ethane)MnCl

There total 14 articles about (CO)3(1,2-bis(diphenylphosphino)ethane)MnCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 10170-69-1
dimanganese decacarbonyl

: 75-09-2
dichloromethane

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 49695-20-7
fac-Mn(CO)3(chloro)(1,2-bis(diphenylphosphino)ethane)

Guidance literature:: In dichloromethane; autoclave (N2, 130°C, 2 h); solvent removal, recrystn. (CH2Cl2/hexane);
DOI:10.1016/s0277-5387(96)00523-2

Reference yield: 98.0%

: Mn₂*6CO*2C₂₆H₂₄P₂ = [Mn₂(CO)6(C₂₆H₂₄P₂)2]

: 75-09-2
dichloromethane

: 49695-20-7
fac-Mn(CO)3(chloro)(1,2-bis(diphenylphosphino)ethane)

Guidance literature:: In dichloromethane; autoclave; solvent removal, recrystn. (CH2Cl2/hexane);
DOI:10.1016/s0277-5387(96)00523-2

Reference yield: 68.0%

: 14100-30-2
pentacarbonylchloromanganese(I)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 49695-20-7
fac-Mn(CO)3(chloro)(1,2-bis(diphenylphosphino)ethane)

Guidance literature:: In chloroform; (N2); stirring (exclusion from light, gentle reflux, ca. 5 h); redn. of volume, addn. to stirred ice cold hexane, filtration, washing (hexane), drying (vac.); elem. anal.;