1,1':2',1''-Terphenyl, 4,4''-dimethoxy-

Base Information

Chemical Name:1,1':2',1''-Terphenyl, 4,4''-dimethoxy-
CAS No.:160538-35-2
Molecular Formula:C20H18O2
Molecular Weight:290.362
Hs Code.:
DSSTox Substance ID:DTXSID50462053
Nikkaji Number:J1.006.977G
Wikidata:Q82286520
Mol file:160538-35-2.mol

Synonyms:1,1':2',1''-Terphenyl, 4,4''-dimethoxy-;160538-35-2;SCHEMBL12715050;DTXSID50462053

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1':2',1''-Terphenyl, 4,4''-dimethoxy-

Chemical Property:

XLogP3:6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:290.130679813
Heavy Atom Count:22
Complexity:282

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=CC=CC=C2C3=CC=C(C=C3)OC

Technology Process of 1,1':2',1''-Terphenyl, 4,4''-dimethoxy-

There total 1 articles about 1,1':2',1''-Terphenyl, 4,4''-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5720-07-0
4-methoxyphenylboronic acid

: 583-53-9
2,3-dibromobenzene

: 74447-76-0
2-bromo-4'-methoxy-1,1'-biphenyl

: 160538-35-2
4,4’’-dimethoxy-1,1′:2′,1’’-terphenyl

Guidance literature:: With palladium diacetate; cesium fluoride; cyclo-octa-1,5-diene; tert-butyl XPhos; In water; for 1.65h; Solvent; Overall yield = 89 percentSpectr.; Milling;
DOI:10.1021/jacs.0c01739

Reference yield: 60.0%

: 160538-35-2
4,4’’-dimethoxy-1,1′:2′,1’’-terphenyl

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 592550-59-9
1,2-bis(3-(diphenylphosphino)-4-methoxyphenyl)benzene

Guidance literature:: 4,4’’-dimethoxy-1,1′:2′,1’’-terphenyl; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; at -40 ℃; for 16h;

chloro-diphenylphosphine; In diethyl ether; hexane; at 0 ℃; for 16h;
DOI:10.1016/S0040-4039(03)00948-1