4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine

Base Information

Chemical Name:4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine
CAS No.:161121-63-7
Molecular Formula:C24H18BrN
Molecular Weight:400.318
Hs Code.:
DSSTox Substance ID:DTXSID40573708
Wikidata:Q82462514
Mol file:161121-63-7.mol

Synonyms:4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine;161121-63-7;DTXSID40573708;2,6-diphenyl-4-(p-bromomethylphenyl)pyridine

Suppliers and Price of 4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine

Chemical Property:

XLogP3:6.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:399.06226
Heavy Atom Count:26
Complexity:378

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC(=CC(=N2)C3=CC=CC=C3)C4=CC=C(C=C4)CBr

Technology Process of 4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine

There total 7 articles about 4-[4-(Bromomethyl)phenyl]-2,6-diphenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3558-65-4
4-(4-methylphenyl)-2,6-diphenylpyridine

: 161121-63-7
4-(4-(bromomethyl)phenyl)-2,6-diphenylpyridine

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 1h; Heating;
DOI:10.1023/A:1020339120810

Reference yield:

: 98-86-2
acetophenone

: 161121-63-7
4-(4-(bromomethyl)phenyl)-2,6-diphenylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 16 percent / 72 percent HClO₄ / toluene / 1 h / Heating

2: 78 percent / 25 percent aq. NH₄OH / 1.5 h / Heating

3: 95 percent / N-bromosuccinimide; benzoyl peroxide / CCl₄ / 1 h / Heating

With ammonium hydroxide; N-Bromosuccinimide; perchloric acid; dibenzoyl peroxide; In tetrachloromethane; toluene;
DOI:10.1023/A:1020339120810

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 161121-63-7
4-(4-(bromomethyl)phenyl)-2,6-diphenylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate; acetic acid / 24 h / 115 °C

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 24 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; ammonium acetate; acetic acid; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1039/c2jm30455d