Technology Process of Carbamic acid, [3-(cyclopropylhydroxymethyl)phenyl]-, phenylmethyl
ester
There total 6 articles about Carbamic acid, [3-(cyclopropylhydroxymethyl)phenyl]-, phenylmethyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
tetrahydrofuran; ethanol;
for 3h;
Ambient temperature;
DOI:10.1021/jm00018a023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 50 percent / fuming 90percent nitric acid / 0.17 h / -10 °C
2: hydrogen / 5percent platinum on carbon / methanol / 5 h / 760 Torr
3: diisopropylethylamine / CH2Cl2 / 4 h / Ambient temperature
4: 96 percent / sodium borohydride / tetrahydrofuran; ethanol / 3 h / Ambient temperature
With
sodium tetrahydroborate; hydrogen; nitric acid; N-ethyl-N,N-diisopropylamine;
platinum on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/jm00018a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen / 5percent platinum on carbon / methanol / 5 h / 760 Torr
2: diisopropylethylamine / CH2Cl2 / 4 h / Ambient temperature
3: 96 percent / sodium borohydride / tetrahydrofuran; ethanol / 3 h / Ambient temperature
With
sodium tetrahydroborate; hydrogen; N-ethyl-N,N-diisopropylamine;
platinum on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
DOI:10.1021/jm00018a023
