2,4-Diphenyl-3,1,5-benzoxadiazepine

Base Information

Chemical Name:2,4-Diphenyl-3,1,5-benzoxadiazepine
CAS No.:16418-23-8
Molecular Formula:C20H14N2O
Molecular Weight:298.344
Hs Code.:
DSSTox Substance ID:DTXSID30557916
Nikkaji Number:J2.047.830F
Mol file:16418-23-8.mol

Synonyms:2,4-Diphenyl-3,1,5-benzoxadiazepine;16418-23-8;DTXSID30557916

Suppliers and Price of 2,4-Diphenyl-3,1,5-benzoxadiazepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,4-Diphenyl-3,1,5-benzoxadiazepine

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:298.110613074
Heavy Atom Count:23
Complexity:416

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NC3=CC=CC=C3N=C(O2)C4=CC=CC=C4

Technology Process of 2,4-Diphenyl-3,1,5-benzoxadiazepine

There total 5 articles about 2,4-Diphenyl-3,1,5-benzoxadiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-88-4
benzoyl chloride

: 95-54-5
1,2-diamino-benzene

: 16418-23-8
2,4-diphenyl-benzo[1,3,6]oxadiazepine

Guidance literature:: With boron trifluoride diethyl etherate; In 1,4-dioxane; Heating;
DOI:10.1016/j.tetlet.2004.03.117

Reference yield: 74.0%

: 744-38-7
1,2-dibenzamidobenzene

: 16418-23-8
2,4-diphenyl-benzo[1,3,6]oxadiazepine

Guidance literature:: With bromine; triethylamine; triphenylphosphine; In dichloromethane; for 1h; Heating;
DOI:10.1007/BF00808308

Reference yield:

: 98-88-4
benzoyl chloride

: 16418-23-8
2,4-diphenyl-benzo[1,3,6]oxadiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NEt₃ / benzene / 2 h / Heating

2: 74 percent / PPh₃, Br₂, NEt₃ / CH₂Cl₂ / 1 h / Heating

With bromine; triethylamine; triphenylphosphine; In dichloromethane; benzene;
DOI:10.1007/BF00808308