1,3,2-Diazaphospholidine, 1,2,3-trimethyl-, 2-oxide

Base Information

• Chemical Name: 1,3,2-Diazaphospholidine, 1,2,3-trimethyl-, 2-oxide
• CAS No.: 16606-18-1
• Molecular Formula: C5H13N2OP
• Molecular Weight: 148.145
• Mol file: 16606-18-1.mol

Synonyms:1,2,3-trimethyl-1,3,2;1,3,2-Diazaphospholidine,1,2,3-trimethyl-,2-oxide;1,2,3-trimethyl-[1,3,2]diazaphospholidine 2-oxide;1,2,3-Trimethyl-2-oxo-1,3,2-diazaphospholidin;1,2,3-Trimethyltetrahydro-1,3,2-diazaphosphole 2-oxide;1,3,2-diazaphospholidine-2-methyl-1,3-dimethyl 2-oxide;

Chemical Property of 1,3,2-Diazaphospholidine, 1,2,3-trimethyl-, 2-oxide

Chemical Property:

• PSA: 33.36000
• LogP: 0.56230

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,2-Diazaphospholidine, 1,2,3-trimethyl-, 2-oxide

There total 3 articles about 1,3,2-Diazaphospholidine, 1,2,3-trimethyl-, 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1,3-dimethyl-2-(2-phenylethoxy)-1,3,2-diazaphospholidine (1108614-42-1) + methyl iodide (74-88-4) → 1,3,2-diazaphospholidine-2-methyl-1,3-dimethyl 2-oxide (16606-18-1) + 2-phenethyl iodide (17376-04-4)

Guidance literature:

In toluene; for 4h; Reflux;

DOI:10.1039/b814452d

Reference yield: 27.0%

pyrrolidine (123-75-1) + 1,3-dimethyl-2-(2-phenylethoxy)-1,3,2-diazaphospholidine (1108614-42-1) + methyl iodide (74-88-4) → 1,3,2-diazaphospholidine-2-methyl-1,3-dimethyl 2-oxide (16606-18-1) + N-(2-phenylethyl)pyrrolidine (6908-75-4)

Guidance literature:

1,3-dimethyl-2-(2-phenylethoxy)-1,3,2-diazaphospholidine; methyl iodide; In toluene; for 4h; Reflux;

pyrrolidine; In toluene; at 20 ℃;

DOI:10.1039/b814452d

Reference yield:

pyrrolidine (123-75-1) + CF3O3S(1-)*C14H23N3O2P(1+) (1108614-40-9) → 1,3,2-diazaphospholidine-2-methyl-1,3-dimethyl 2-oxide (16606-18-1) + 2-phenyl-1,3-oxazoline (7127-19-7)

Guidance literature:

DOI:10.1039/b814452d

upstream raw materials:

pyrrolidine

CF₃O₃S^(1-)*C₁₄H₂₃N₃O₂P⁽¹⁺⁾

1,3-dimethyl-2-(2-phenylethoxy)-1,3,2-diazaphospholidine

methyl iodide

Downstream raw materials:

1,1-Diphenylethylene

methylenecyclopentane

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