3-Bromo-5-methoxyaniline

Base Information

Chemical Name:3-Bromo-5-methoxyaniline
CAS No.:16618-68-1
Molecular Formula:C7H8BrNO
Molecular Weight:202.051
Hs Code.:2922299090
European Community (EC) Number:692-479-3
DSSTox Substance ID:DTXSID40566731
Wikidata:Q72446021
Mol file:16618-68-1.mol

Synonyms:3-Bromo-5-methoxyaniline;16618-68-1;Benzenamine, 3-bromo-5-methoxy-;MFCD11878497;3-BROMO-5-METHOXYBENZENAMINE;3-Amino-5-bromoanisole;5-Bromo-m-anisidine;3-bromo-5-methoxybenzeneamine;SCHEMBL378876;3-Bromo-5-methoxyaniline 98%;DTXSID40566731;FHUSNGUPJXGLPL-UHFFFAOYSA-N;BCP20491;CS-B0549;3-BROMO-5-METHYLOXYBENZENAMINE;AKOS016001973;AB65032;PS-5038;SY042906;EN300-67112;A882346;AU-004/40000567;Z1065885484

Suppliers and Price of 3-Bromo-5-methoxyaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Bromo-5-methoxyaniline
50mg
$ 60.00

SynQuest Laboratories
3-Bromo-5-methoxyaniline 98%
5 g
$ 395.00

SynQuest Laboratories
3-Bromo-5-methoxyaniline 98%
1 g
$ 125.00

Oakwood
3-Bromo-5-methoxyaniline
1g
$ 40.00

Oakwood
3-Bromo-5-methoxyaniline
5g
$ 120.00

Oakwood
3-Bromo-5-methoxyaniline
250mg
$ 20.00

Oakwood
3-Bromo-5-methoxyaniline
25g
$ 360.00

Oakwood
3-Bromo-5-methoxyaniline
100g
$ 900.00

Matrix Scientific
3-Bromo-5-methoxyaniline 97%
1g
$ 260.00

Crysdot
3-Bromo-5-methoxyaniline 98%
100g
$ 891.00

Total 37 raw suppliers

Chemical Property of 3-Bromo-5-methoxyaniline

Chemical Property:

Boiling Point:285.8±20.0℃ (760 Torr)
PKA:3.10±0.10(Predicted)
Flash Point:126.7±21.8℃
PSA：35.25000
Density:1.531±0.06 g/cm3 (20 oC 760 Torr)
LogP:2.62110
Storage Temp.:2-8°C(protect from light)
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:200.97893
Heavy Atom Count:10
Complexity:110

Purity/Quality:

99%, ^*data from raw suppliers

3-Bromo-5-methoxyaniline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC(=C1)N)Br

Technology Process of 3-Bromo-5-methoxyaniline

There total 4 articles about 3-Bromo-5-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

: 16618-67-0
3-bromo-5-nitroanisole

: 16618-68-1
3-bromo-5-methoxyaminobenzene

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; acetone; at 20 ℃; for 3h;

Reference yield:

: 99-65-0
meta-dinitrobenzene

: 16618-68-1
3-bromo-5-methoxyaminobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; N-Bromosuccinimide / 1 h / 85 °C

2: methanol / 20 °C

3: ammonium chloride; iron / methanol; water / 95 °C

With N-Bromosuccinimide; sulfuric acid; iron; ammonium chloride; In methanol; water;
DOI:10.1021/jm500432n

Reference yield:

: 18242-39-2
3,5-dinitrobromobenzene

: 16618-68-1
3-bromo-5-methoxyaminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 20 °C

2: ammonium chloride; iron / methanol; water / 95 °C

With iron; ammonium chloride; In methanol; water;
DOI:10.1021/jm500432n