17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate

Base Information

Chemical Name:17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate
CAS No.:77573-84-3
Molecular Formula:C15H28 O8
Molecular Weight:336.383
Hs Code.:2916129000
European Community (EC) Number:278-725-9
DSSTox Substance ID:DTXSID00228247
Nikkaji Number:J309.412J
Wikidata:Q83108214
Mol file:77573-84-3.mol

Synonyms:77573-84-3;17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate;EINECS 278-725-9;SCHEMBL259313;DTXSID00228247;C15H28O8;C15-H28-O8;Acrylic acid 17-hydroxy-3,6,9,12,15-pentaoxaheptadecane-1-yl ester

Suppliers and Price of 17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:427.981°C at 760 mmHg
Flash Point:144.743°C
PSA：92.68000
Density:1.106g/cm³
LogP:-0.20910
XLogP3:-0.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:19
Exact Mass:336.17841785
Heavy Atom Count:23
Complexity:272

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC(=O)OCCOCCOCCOCCOCCOCCO

Technology Process of 17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate

There total 2 articles about 17-Hydroxy-3,6,9,12,15-pentaoxaheptadecyl acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 2615-15-8
pentaethylene glycol

: 814-68-6,25189-84-8
acryloyl chloride

: 77573-84-3,9051-31-4
Acrylic acid 2-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1080/00397919708004135

Reference yield:

: 2615-15-8
pentaethylene glycol

: 140-88-5,9003-32-1
ethyl acrylate

: 77573-84-3,9051-31-4
Acrylic acid 2-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester

Guidance literature:: With di(n-butyl)tin oxide; In toluene; for 10h; Dean-Stark; Reflux;

Reference yield:

: 77573-84-3,9051-31-4
Acrylic acid 2-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethyl ester

: C₂₂H₃₂O₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere; Cooling with ice

2: potassium carbonate / N,N-dimethyl-formamide / 15 h / 90 °C

3: dihydrogen peroxide; sodium chlorite; sodium dihydrogenphosphate dihydrate / methanol; water / 5 h / 45 °C

With pyridine; sodium chlorite; sodium dihydrogenphosphate dihydrate; dihydrogen peroxide; potassium carbonate; In methanol; dichloromethane; water; N,N-dimethyl-formamide;