2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane

Base Information

Chemical Name:2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane
CAS No.:16892-66-3
Molecular Formula:C36H30S3Sn3
Molecular Weight:914.962
Hs Code.:
DSSTox Substance ID:DTXSID80586897
Wikidata:Q82479121
Mol file:16892-66-3.mol

Synonyms:DTXSID80586897;16892-66-3;2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane;2,2,4,4,6,6-hexaphenyl-1 ,3,5-trithia-2 ,4,6-tristannacyclohexane

Suppliers and Price of 2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane

Chemical Property:

Melting Point:181-184 °C
PSA：75.90000
LogP:6.51060
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:915.85698
Heavy Atom Count:42
Complexity:651

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Sn]2(S[Sn](S[Sn](S2)(C3=CC=CC=C3)C4=CC=CC=C4)(C5=CC=CC=C5)C6=CC=CC=C6)C7=CC=CC=C7

Technology Process of 2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane

There total 4 articles about 2,2,4,4,6,6-Hexaphenyl-1,3,5,2,4,6-trithiatristanninane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: sodiumsulfide nonahydrate

: 1135-99-5
diphenyltin(IV) dichloride

: 16892-66-3
2,2,4,4,6,6-hexaphenylcyclotri(stannathiane)

Guidance literature:: In ethanol; water; dropwise addn. of a soln. of the tin chloride in ethanol to a soln. of the sulfide in water; filtration after 15 min, washing (water), drying over P4O10, recrystn. (ethanol), elem. anal.;

Reference yield: 70.0%

: lithium sulfide

: 1135-99-5
diphenyltin(IV) dichloride

: 16892-66-3
2,2,4,4,6,6-hexaphenylcyclotri(stannathiane)

Guidance literature:: In tetrahydrofuran; toluene; byproducts: LiCl; toluene soln. of Ph2SnCl2 was added to THF soln. of Li2S, mixt. was stirred overnight; solvent was removed, toluene was added, mixt. was filtered, filtrate wasevapd., ppt. was recrystd. from toluene/hexane; NMR, XRD;
DOI:10.1016/S0022-328X(02)01690-X