4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

Base Information

Chemical Name:4-chloro-N-(3-methoxyphenyl)benzenesulfonamide
CAS No.:16936-96-2
Molecular Formula:C₁₃H₁₂ClNO₃S
Molecular Weight:297.762
Hs Code.:
Mol file:16936-96-2.mol

Synonyms:4-Chloro-N-(3-methoxy-phenyl)-benzenesulfonamide;4-Chlor-benzolsulfon-N-(3-methoxy-phenyl)-amid;

Suppliers and Price of 4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

Chemical Property:

Melting Point:65 °C
PSA：63.78000
LogP:4.30320

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

There total 5 articles about 4-chloro-N-(3-methoxyphenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 16936-96-2
4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2006.05.091

Reference yield:

: 2-[(4-chlorophenyl)sulfonamido]-6-methoxybenzoic acid

: 16936-96-2
4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

Guidance literature:: With palladium diacetate; In 1,2-dichloro-ethane; at 120 ℃; for 12h;
DOI:10.1002/chem.201500331

Reference yield:

: 4547-68-6
p-chlorobenzenesulfonyl azide

: 16936-96-2
4-chloro-N-(3-methoxyphenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide; lithium acetate / 1,2-dichloro-ethane / 24 h / 50 °C

2: palladium diacetate / 1,2-dichloro-ethane / 12 h / 120 °C

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; lithium acetate; palladium diacetate; silver(I) triflimide; In 1,2-dichloro-ethane;
DOI:10.1002/chem.201500331