Phenylalanine, a-methyl-4-nitro-, phenylmethyl ester

Base Information

Chemical Name:Phenylalanine, a-methyl-4-nitro-, phenylmethyl ester
CAS No.:169689-26-3
Molecular Formula:C17H18N2O4
Molecular Weight:314.341
Hs Code.:

Synonyms:

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Chemical Property of Phenylalanine, a-methyl-4-nitro-, phenylmethyl ester

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Technology Process of Phenylalanine, a-methyl-4-nitro-, phenylmethyl ester

There total 12 articles about Phenylalanine, a-methyl-4-nitro-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2-{[1-(5-Benzyloxymethyl-3-methoxy-2-methyl-pyridin-4-yl)-meth-(E)-ylidene]-amino}-propionic acid benzyl ester

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 169689-33-2
5-(benzyloxymethyl)-3-methoxy-2-methylpyridine-4-carbaldehyde

: 169689-26-3
benzyl 2-amino-2-methyl-3-(4-nitrophenyl)propanoate

Guidance literature:: With hydrogenchloride; sodium hydroxide; Et₃NBn⁽¹⁺⁾Cl^(1-); Product distribution; multistep reaction; other α-imino ester, var. alkali hydroxide, with and without additives;
DOI:10.1246/cl.1995.487

Reference yield: 44.0%

: 100-11-8
1-bromomethyl-4-nitro-benzene

: (S)-2-{[1-{5-Benzyloxymethyl-3-[(S)-2-methoxy-3-(naphthalen-1-ylmethoxy)-propoxy]-2-methyl-pyridin-4-yl}-meth-(E)-ylidene]-amino}-propionic acid benzyl ester

: 169689-26-3
benzyl 2-amino-2-methyl-3-(4-nitrophenyl)propanoate

: 252272-60-9
(S)-5-(benzyloxymethyl)-3-[2-methoxy-3-(1-naphthylmethoxy)propoxy]-2-methylpyridine-4-carbaldehyde

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 10h;
DOI:10.1016/S0040-4020(99)00708-5

Reference yield:

: 17831-01-5,17831-02-6,46229-47-4
DL-alanine benzyl ester

: 169689-26-3
benzyl 2-amino-2-methyl-3-(4-nitrophenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / benzene / 3 h / Heating

2: 1.) LiOH / 1.) CH₂Cl₂, RT, 5 min, 2.) CH₂Cl₂, RT, 3 h

3: 5percent aq. HCl / ethyl acetate / 0.08 h / Ambient temperature

With hydrogenchloride; lithium hydroxide; In ethyl acetate; benzene;
DOI:10.1016/0040-4020(96)00704-1