1H-Indole-4-carboxylic acid, 1-[(dimethylamino)carbonyl]-3-[4-[(2-methyl-1H-imidazo[4,5-c]pyridin-1- yl)methyl]benzoyl]-, phenylmethyl ester

Base Information

Chemical Name:1H-Indole-4-carboxylic acid, 1-[(dimethylamino)carbonyl]-3-[4-[(2-methyl-1H-imidazo[4,5-c]pyridin-1- yl)methyl]benzoyl]-, phenylmethyl ester
CAS No.:170498-43-8
Molecular Formula:C₃₄H₂₉N₅O₄
Molecular Weight:571.635
Hs Code.:
Mol file:170498-43-8.mol

1H-Indole-4-carboxylic acid,
1-[(dimethylamino)carbonyl]-3-[4-[(2-methyl-1H-imidazo[4,5-c]pyridin-1-
yl)methyl]benzoyl]-, phenylmethyl ester

Synonyms:

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Chemical Property of 1H-Indole-4-carboxylic acid, 1-[(dimethylamino)carbonyl]-3-[4-[(2-methyl-1H-imidazo[4,5-c]pyridin-1- yl)methyl]benzoyl]-, phenylmethyl ester

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Technology Process of 1H-Indole-4-carboxylic acid, 1-[(dimethylamino)carbonyl]-3-[4-[(2-methyl-1H-imidazo[4,5-c]pyridin-1- yl)methyl]benzoyl]-, phenylmethyl ester

There total 7 articles about 1H-Indole-4-carboxylic acid, 1-[(dimethylamino)carbonyl]-3-[4-[(2-methyl-1H-imidazo[4,5-c]pyridin-1- yl)methyl]benzoyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2124-55-2
1H-indole-4-carboxylic acid

: 170498-43-8
1-N,N-dimethylcarbamoyl-4-benzyloxycarbonyl-3-{4-[(1H-2-methylimidazo[4.5-c]pyrid-1-yl)methyl]benzoyl}indole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaHCO₃ / 1.) DMF, RT, 10 min, 2.) DMF, RT, 48 h

2: 1.) EtMgBr, 2.) ZnCl₂

3: 1.) NaH / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 1 h

4: 1.) NaBr, 2.) DMPU / 1.) THF, RT, 1 h, 2.) THF, RT, 3 h

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; ethylmagnesium bromide; sodium hydride; sodium hydrogencarbonate; sodium bromide; zinc(II) chloride;
DOI:10.1021/jm970389+

Reference yield:

: 100-39-0
benzyl bromide

: 170498-43-8
1-N,N-dimethylcarbamoyl-4-benzyloxycarbonyl-3-{4-[(1H-2-methylimidazo[4.5-c]pyrid-1-yl)methyl]benzoyl}indole

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaHCO₃ / 1.) DMF, RT, 10 min, 2.) DMF, RT, 48 h

2: 1.) EtMgBr, 2.) ZnCl₂

3: 1.) NaH / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 1 h

4: 1.) NaBr, 2.) DMPU / 1.) THF, RT, 1 h, 2.) THF, RT, 3 h

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; ethylmagnesium bromide; sodium hydride; sodium hydrogencarbonate; sodium bromide; zinc(II) chloride;
DOI:10.1021/jm970389+

Reference yield:

: 84401-11-6
benzyl indole-4-carboxylate

: 170498-43-8
1-N,N-dimethylcarbamoyl-4-benzyloxycarbonyl-3-{4-[(1H-2-methylimidazo[4.5-c]pyrid-1-yl)methyl]benzoyl}indole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) EtMgBr, 2.) ZnCl₂

2: 1.) NaH / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, 1 h

3: 1.) NaBr, 2.) DMPU / 1.) THF, RT, 1 h, 2.) THF, RT, 3 h

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; ethylmagnesium bromide; sodium hydride; sodium bromide; zinc(II) chloride;
DOI:10.1021/jm970389+