Technology Process of 3-Chloroacridine
There total 18 articles about 3-Chloroacridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; benzylamine;
at 120 ℃;
for 16h;
Inert atmosphere;
Glovebox;
Schlenk technique;
Sealed tube;
DOI:10.1080/00397911.2018.1448418
- Guidance literature:
-
With
trifluoroacetic acid;
at 80 ℃;
for 10h;
Inert atmosphere;
- Guidance literature:
-
3-chloro-10H-dibenzo[b,e]iodinin-5-ium trifluoromethanesulfonate;
With
sodium azide; triphenylphosphine;
In
N,N-dimethyl acetamide; water;
at 120 ℃;
for 0.5h;
Inert atmosphere;
Schlenk technique;
With
copper(I) thiophene-2-carboxylate; caesium carbonate;
In
N,N-dimethyl acetamide; water;
at 120 ℃;
for 48h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/acs.orglett.7b03564
