1-Methoxy-3-(trimethylstannyl)benzene

Base Information

• Chemical Name: 1-Methoxy-3-(trimethylstannyl)benzene
• CAS No.: 17113-78-9
• Molecular Formula: C10H16OSn
• Molecular Weight: 270.946
• Hs Code.: 2931900090
• Mol file: 17113-78-9.mol

Synonyms:Stannane,(3-methoxyphenyl)trimethyl;Stannane,(m-methoxyphenyl)trimethyl;1-Methoxy-3-(trimethylstannyl)benzene;

Chemical Property of 1-Methoxy-3-(trimethylstannyl)benzene

Chemical Property:

• PSA: 9.23000
• LogP: 2.48750

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Methoxy-3-(trimethylstannyl)benzene

There total 9 articles about 1-Methoxy-3-(trimethylstannyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

O,O-diethyl O-3-methoxyphenyl phosphate (13538-32-4) + trimethylstannyl sodium (16643-09-7) → 3-trimethylstannylanisole (17113-78-9)

Guidance literature:

In ammonia; Irradiation (UV/VIS); irradiated for 4 h;

DOI:10.1016/j.jorganchem.2005.05.023

Reference yield: 78.0%

trimethyltin(IV)chloride (1066-45-1) + (3-methoxyphenyl)magnesium bromide (36282-40-3) → 3-trimethylstannylanisole (17113-78-9)

Guidance literature:

In diethyl ether; refluxing for 2 h;;

DOI:10.1016/S0022-328X(00)83182-4

Reference yield: 76.0%

trimethyltin bromide (1066-44-0) → 3-trimethylstannylanisole (17113-78-9)

Guidance literature:

In diethyl ether;

upstream raw materials:

3-methoxyphenyl bromide

trimethyltin(IV)chloride

O,O-diethyl O-3-methoxyphenyl phosphate

trimethylstannyl sodium

Downstream raw materials:

2-(3-Methoxy-phenyl)-4-methyl-nicotinic acid ethyl ester

m-Methoxybenzenesulfonyl chloride

3-methoxybenzophenone

trimethyltin(IV)chloride

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