Tert-butyl 2-bromophenethylcarbamate

Base Information

Chemical Name:Tert-butyl 2-bromophenethylcarbamate
CAS No.:171663-06-2
Molecular Formula:C13H18BrNO2
Molecular Weight:300.195
Hs Code.:
European Community (EC) Number:871-791-5
DSSTox Substance ID:DTXSID90598800
Nikkaji Number:J1.326.038I
Wikidata:Q82494603
Mol file:171663-06-2.mol

Synonyms:TERT-BUTYL 2-BROMOPHENETHYLCARBAMATE;171663-06-2;TERT-BUTYL N-[2-(2-BROMOPHENYL)ETHYL]CARBAMATE;tert-butyl2-bromophenethylcarbamate;tert-butyl [2-(2-bromophenyl)ethyl]carbamate;SCHEMBL1343816;DTXSID90598800;CCLKBQZVNSHZLO-UHFFFAOYSA-N;WGA66306;MFCD11042236;AKOS027255734;AB62835;CS-W004183;AS-54921;DB-210284;Tert-butyl 2-(2-bromophenyl)ethylcarbamate;EN300-176332;W11073;[2-(2-BROMO-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER

Suppliers and Price of Tert-butyl 2-bromophenethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl2-bromophenethylcarbamate 95+%
5g
$ 456.00

Chemenu
tert-Butyl2-bromophenethylcarbamate 95%
5g
$ 426.00

American Custom Chemicals Corporation
TERT-BUTYL-2-BROMOPHENETHYLCARBAMATE 95.00%
1G
$ 278.25

American Custom Chemicals Corporation
TERT-BUTYL-2-BROMOPHENETHYLCARBAMATE 95.00%
10G
$ 5595.98

American Custom Chemicals Corporation
TERT-BUTYL-2-BROMOPHENETHYLCARBAMATE 95.00%
5G
$ 4204.20

Alichem
tert-Butyl2-bromophenethylcarbamate
5g
$ 446.88

AK Scientific
tert-butylN-[2-(2-bromophenyl)ethyl]carbamate
250mg
$ 155.60

AK Scientific
tert-butylN-[2-(2-bromophenyl)ethyl]carbamate
100mg
$ 131.60

Acrotein
tert-Butyl2-bromophenethylcarbamate 97%
0.5g
$ 119.16

Total 4 raw suppliers

Chemical Property of Tert-butyl 2-bromophenethylcarbamate

Chemical Property:

Boiling Point:385.8±25.0 °C(Predicted)
PKA:12.52±0.46(Predicted)
PSA：41.82000
Density:1.286±0.06 g/cm3(Predicted)
LogP:3.72070
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:299.05209
Heavy Atom Count:17
Complexity:250

Purity/Quality:

98%min ^*data from raw suppliers

tert-Butyl2-bromophenethylcarbamate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCCC1=CC=CC=C1Br

Technology Process of Tert-butyl 2-bromophenethylcarbamate

There total 2 articles about Tert-butyl 2-bromophenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 65185-58-2
2-(2-bromophenyl)ethanamine

: 171663-06-2
N-(tert-butoxycarbonyl)-2-(2-bromophenyl)-ethylamine

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; at 0 - 20 ℃;
DOI:10.1021/jm0606600

Reference yield: 89.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 19472-74-3
2-(2-bromophenyl)acetonitrile

: 171663-06-2
N-(tert-butoxycarbonyl)-2-(2-bromophenyl)-ethylamine

Guidance literature:: di-tert-butyl dicarbonate; 2-(2-bromophenyl)acetonitrile; With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; at 0 - 20 ℃; for 1.5h;

With diethylamine; In methanol; for 0.5h;
DOI:10.1021/jo102452d

Reference yield: 99.0%

: 74-88-4
methyl iodide

: 171663-06-2
N-(tert-butoxycarbonyl)-2-(2-bromophenyl)-ethylamine

: 500876-19-7
N-Boc-N-methyl-N-(2-(2-bromophenyl)ethyl)amine

Guidance literature:: N-(tert-butoxycarbonyl)-2-(2-bromophenyl)-ethylamine; With sodium hydride; In tetrahydrofuran; for 0.166667h;

methyl iodide; In tetrahydrofuran; at 40 ℃; for 24h;
DOI:10.1021/jo8016428