Cyclopropanecarboxamide, 2-[(1S)-1-aminopropyl]-N,N-diethyl-1-phenyl-, (1S,2R)-

Base Information

Chemical Name:Cyclopropanecarboxamide, 2-[(1S)-1-aminopropyl]-N,N-diethyl-1-phenyl-, (1S,2R)-
CAS No.:171889-07-9
Molecular Formula:C17H26N2O
Molecular Weight:274.406
Hs Code.:

Synonyms:

Suppliers and Price of Cyclopropanecarboxamide, 2-[(1S)-1-aminopropyl]-N,N-diethyl-1-phenyl-, (1S,2R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclopropanecarboxamide, 2-[(1S)-1-aminopropyl]-N,N-diethyl-1-phenyl-, (1S,2R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropanecarboxamide, 2-[(1S)-1-aminopropyl]-N,N-diethyl-1-phenyl-, (1S,2R)-

There total 23 articles about Cyclopropanecarboxamide, 2-[(1S)-1-aminopropyl]-N,N-diethyl-1-phenyl-, (1S,2R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 171889-11-5
(1S,2R)-2-((S)-1-Amino-allyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

: 171889-07-9
(1S,2R)-1-phenyl-2-[(S)-1-aminopropyl]-N,N-diethylcyclopropanecarboxamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 1.5h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm960495w

Reference yield: 74.0%

: 779308-86-0
(1S,2R)-2-((R)-1-Amino-prop-2-ynyl)-1-phenyl-cyclopropanecarboxylic acid diethylamide

: 171889-07-9
(1S,2R)-1-phenyl-2-[(S)-1-aminopropyl]-N,N-diethylcyclopropanecarboxamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm980238m

Reference yield:

: 172016-00-1
(1S,2R)-2-Formyl-1-phenyl-cyclopropanecarboxylic acid diethylamide

: 171889-07-9
(1S,2R)-1-phenyl-2-[(S)-1-aminopropyl]-N,N-diethylcyclopropanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / 20 °C

2.1: MgBr₂ / diethyl ether; tetrahydrofuran / 0.5 h / 20 °C

2.2: 80 percent / diethyl ether; tetrahydrofuran / 8 h / -78 °C

3.1: H₂ / 10percent Pd/C / methanol / 72 h / 1551.49 Torr

With 4 A molecular sieve; hydrogen; magnesium bromide; 10percent Pd/C; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1039/b008230i