Spiro[bicyclo[2.2.1]heptane-2,2'-[1,3]dioxolane]

Base Information

• Chemical Name: Spiro[bicyclo[2.2.1]heptane-2,2'-[1,3]dioxolane]
• CAS No.: 172-67-8
• Molecular Formula: C9H14O2
• Molecular Weight: 154.209
• Hs Code.: 2932999099
• NSC Number: 120509
• DSSTox Substance ID: DTXSID00298086
• Mol file: 172-67-8.mol

Synonyms:172-67-8;spiro[1,3-dioxolane-2,2'-bicyclo[2.2.1]heptane];Spiro[bicyclo[2.2.1]heptane-2,2-[1,3]dioxolane] (9CI);spiro[bicyclo[2.2.1]heptane-2,2'-[1,3]dioxolane];NSC120509;SCHEMBL22681046;DTXSID00298086;NSC-120509;Spiro[1,3-dioxolane-2,2'-norbornane]

Chemical Property of Spiro[bicyclo[2.2.1]heptane-2,2'-[1,3]dioxolane]

Chemical Property:

• Vapor Pressure: 0.437mmHg at 25°C
• Boiling Point: 201.5oC at 760 mmHg
• Flash Point: 71.9oC
• PSA: 18.46000
• Density: 1.13g/cm3
• LogP: 1.54950
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 154.099379685
• Heavy Atom Count: 11
• Complexity: 172

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC2CC1CC23OCCO3

Technology Process of Spiro[bicyclo[2.2.1]heptane-2,2'-[1,3]dioxolane]

There total 2 articles about Spiro[bicyclo[2.2.1]heptane-2,2'-[1,3]dioxolane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Norbornan-2-on (497-38-1) + ethylene glycol (107-21-1) → Norcampher-ethylenketal (172-67-8)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; Heating;

DOI:10.1021/jo00084a021

Reference yield:

→ norbornanone ethylene glycol ketal (172-67-8)

Guidance literature:

Norcampher, Ethylenglykol, Benzol, p-Toluolsulfonsaeure, Δ;

DOI:10.1139/v66-230

Reference yield: 11.0%

Norcampher-ethylenketal (172-67-8) + 1,2,4,5-tetracyanobenzene (712-74-3) → 2-Hydroxyethyl cyclopentaneacetate + trans-2-Hydroxyethyl 3-<(2,4,5-tricyanophenyl)methyl>cyclopentanecarboxylate + trans-2-Hydroxyethyl 3-(2,4,5-tricyanophenyl)cyclopentaneacetate + cis-2-Hydroxyethyl 3-(2,4,5-tricyanophenyl)cyclopentaneacetate

Guidance literature:

With water; In acetonitrile; for 1h; Yields of byproduct given; Irradiation;

DOI:10.1021/jo00084a021

upstream raw materials:

Norbornan-2-on

ethylene glycol

Downstream raw materials:

2-norbornanone

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