Benzoic acid, 5-chloro-2-[methyl[3-[methyl[3-(trifluoromethyl)phenyl]amino]-1-oxo-3-thi oxopropyl]amino]-, ethyl ester

Base Information

Chemical Name:Benzoic acid, 5-chloro-2-[methyl[3-[methyl[3-(trifluoromethyl)phenyl]amino]-1-oxo-3-thi oxopropyl]amino]-, ethyl ester
CAS No.:172896-74-1
Molecular Formula:C21H20ClF3N2O3S
Molecular Weight:472.916
Hs Code.:
Mol file:172896-74-1.mol

Synonyms:

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Chemical Property of Benzoic acid, 5-chloro-2-[methyl[3-[methyl[3-(trifluoromethyl)phenyl]amino]-1-oxo-3-thi oxopropyl]amino]-, ethyl ester

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Technology Process of Benzoic acid, 5-chloro-2-[methyl[3-[methyl[3-(trifluoromethyl)phenyl]amino]-1-oxo-3-thi oxopropyl]amino]-, ethyl ester

There total 2 articles about Benzoic acid, 5-chloro-2-[methyl[3-[methyl[3-(trifluoromethyl)phenyl]amino]-1-oxo-3-thi oxopropyl]amino]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 172896-87-6
N-(3-trifluoromethylphenyl)-N-methylthiocarbamoylacetic acid

: 172896-37-6
ethyl 5-chloro-2-(methylamino)benzoate

: 172896-74-1
ethyl 5-chloro-2-(methyl-{2-[methyl-(3-trifluoromethylphenyl)thiocarbamoyl]-acetyl}-amino)-benzoate

Guidance literature:: With pyridine; 4 A molecular sieve; pivaloyl chloride; In dichloromethane; at -20 - 20 ℃;
DOI:10.1002/jhet.5570390427

Reference yield:

: 64-17-5
ethanol

: 14529-12-5
6-chloro-N-methylisatoic anhydride

: 172896-87-6
N-(3-trifluoromethylphenyl)-N-methylthiocarbamoylacetic acid

: 172896-74-1
ethyl 5-chloro-2-(methyl-{2-[methyl-(3-trifluoromethylphenyl)thiocarbamoyl]-acetyl}-amino)-benzoate

Guidance literature:: ethanol; 6-chloro-N-methylisatoic anhydride; With sodium ethanolate; Heating;

N-(3-trifluoromethylphenyl)-N-methylthiocarbamoylacetic acid; With pyridine; pivaloyl chloride; In dichloromethane; at 20 ℃;
DOI:10.1016/S0960-894X(02)00377-3