(NO₂C₆H₃(CHNC₆H₄CH₃)(NSO₂C₆H₄Br))2Ni

Base Information

• Chemical Name: (NO₂C₆H₃(CHNC₆H₄CH₃)(NSO₂C₆H₄Br))2Ni
• CAS No.: 134398-97-3
• Molecular Formula: C₄₀H₃₀Br₂N₆NiO₈S₂
• Molecular Weight: 1005.34
• Mol file: 134398-97-3.mol

Synonyms:

Chemical Property of (NO₂C₆H₃(CHNC₆H₄CH₃)(NSO₂C₆H₄Br))2Ni

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (NO₂C₆H₃(CHNC₆H₄CH₃)(NSO₂C₆H₄Br))2Ni

There total 1 articles about (NO₂C₆H₃(CHNC₆H₄CH₃)(NSO₂C₆H₄Br))2Ni which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-nitro-2-[N-(p-toluenesulfonyl)amino]benzaldehyde (39119-35-2) + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) + 4-bromo-aniline (106-40-1) → (NO2C6H3(CHNC6H4CH3)(NSO2C6H4Br))2Ni (134398-97-3)

Guidance literature:

In 1,4-dioxane; ethanol; mixing hot dioxane solns. of the aldehyde and the amine and ethanolic soln. of Ni(ac)2; cooling, filtn., washing with EtOH, drying in a vacuum dessicator at 150°C, elem. anal.;

upstream raw materials:

5-nitro-2-[N-(p-toluenesulfonyl)amino]benzaldehyde

nickel diacetate

4-bromo-aniline