Ethanone, 2-[(4-methylphenyl)sulfinyl]-1-phenyl-

Base Information

• Chemical Name: Ethanone, 2-[(4-methylphenyl)sulfinyl]-1-phenyl-
• CAS No.: 17530-89-1
• Molecular Formula: C15H14O2S
• Molecular Weight: 258.341
• DSSTox Substance ID: DTXSID30458050
• Nikkaji Number: J316.220F
• Mol file: 17530-89-1.mol

Synonyms:17530-89-1;Ethanone, 2-[(4-methylphenyl)sulfinyl]-1-phenyl-;2-(4-methylphenyl)sulfinyl-1-phenylethanone;DTXSID30458050;1-Phenyl-2-(p-tolyl)sulfinylethanone;AKOS013962462;(+)-(r)-a-(p-tolylsulfinyl)-acetophenone;2-[(4-methylphenyl)sulfinyl]-1-phenylethanone

Chemical Property of Ethanone, 2-[(4-methylphenyl)sulfinyl]-1-phenyl-

Chemical Property:

• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 258.07145086
• Heavy Atom Count: 18
• Complexity: 300

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)CC(=O)C2=CC=CC=C2

Technology Process of Ethanone, 2-[(4-methylphenyl)sulfinyl]-1-phenyl-

There total 11 articles about Ethanone, 2-[(4-methylphenyl)sulfinyl]-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-phenyl-2-(p-tolylthio)ethanone (33046-45-6) → p-tolyl phenacyl sulphoxide (17530-89-1)

Guidance literature:

With Oxone; aluminium trichloride; for 0.5h; Heating;

Reference yield: 98.0%

1-phenyl-2-(toluene-4-sulfinyl)-ethanone oxime → p-tolyl phenacyl sulphoxide (17530-89-1)

Guidance literature:

With benzyltriphenylphosphonium peroxodisulfate; In acetonitrile; for 0.966667h; Heating;

DOI:10.1080/10426500008042103

Reference yield: 95.0%

N,N-dimethyl-N'-[1-phenyl-2-(toluene-4-sulfinyl)-ethylidene]-hydrazine → p-tolyl phenacyl sulphoxide (17530-89-1)

Guidance literature:

With benzyltriphenylphosphonium peroxodisulfate; In acetonitrile; for 1h; Heating;

DOI:10.1080/10426500008042103

upstream raw materials:

1-phenyl-2-(p-tolylsulfinyl)ethan-1-ol

sodium p-thiocresolate

1-chloroacetophenone

methyl p-toluene sulfinate

Downstream raw materials:

1-phenyl-2-(p-tolylthio)ethanone

benzoyl(4-methylphenylthio)methyl acetate

2-oxo-1-phenyl-2-(phenylamino)ethyl acetate

(RS)-mandelamide