gallane, dimethylbenzylamine adduct

Base Information

Chemical Name:gallane, dimethylbenzylamine adduct
CAS No.:192209-80-6
Molecular Formula:C₉H₁₆GaN
Molecular Weight:207.956
Hs Code.:

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Chemical Property of gallane, dimethylbenzylamine adduct

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Technology Process of gallane, dimethylbenzylamine adduct

There total 1 articles about gallane, dimethylbenzylamine adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13450-90-3
Gallium trichloride

: 1875-92-9
N,N-dimethylbenzylamine hydrochloride

: lithium hydride

: 192209-80-6
gallane, dimethylbenzylamine adduct

Guidance literature:: In diethyl ether; Ar-atmosphere; slow addn. of GaCl3 to excess LiH at -80°C, stirring with warming to room temp. over 12 h, filtration, addn. of BzNMe2*HCl(-80°C), stirring at room temp. for 2 h; filtration, concn. (vac.), crystn. (-25°C, 24 h); elem. anal.;
DOI:10.1016/s0020-1693(97)05465-0