Methylphenoxychloraluminium

Base Information

• Chemical Name: Methylphenoxychloraluminium
• CAS No.: 111399-50-9
• Molecular Formula: C₇H₈AlClO
• Molecular Weight: 170.574
• Mol file: 111399-50-9.mol

Synonyms:

Chemical Property of Methylphenoxychloraluminium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Methylphenoxychloraluminium

There total 2 articles about Methylphenoxychloraluminium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylaluminum dichloride (917-65-7) + methoxybenzene (100-66-3) → Methylphenoxychloraluminium (111399-50-9)

Guidance literature:

In neat (no solvent); byproducts: MeCl, CH4, C2H4; PhOMe was introduced very slowly to the stirred MeAlCl2 (in 1:1 molar ratio) at about -10°C, mixt. was heated at 130°C for 6 h; 85 % of gases are evolved, MeCl/CH4/C2H4 = 95:4:traces;

DOI:10.1016/S0022-328X(00)99359-8

Reference yield:

→ Methylphenoxychloraluminium (111399-50-9)

Guidance literature:

Phenol, entspr. Organoaluminiumverb.;

DOI:10.1016/S0022-328X(00)86267-1

upstream raw materials:

methylaluminum dichloride

methoxybenzene

Refernces