(3-glycidoxypropyl)-1,1,3,3-tetramethyldisiloxane

Base Information

• Chemical Name: (3-glycidoxypropyl)-1,1,3,3-tetramethyldisiloxane
• CAS No.: 17980-29-9
• Molecular Formula: C10H24O3Si2
• Molecular Weight: 248.47
• Mol file: 17980-29-9.mol

Synonyms:1-Pentanone,1-(3-furanyl)-4-methyl;3-(3-Methylpentanoyl)furan;1-(3-furyl)-4-methylpentan-1-one;(1,1,3,3-tetramethyldisiloxane-3-ylpropyl) glycidyl ether;perilla ketone;(3-glycidoxypropyl)tetramethyldisiloxane;Purple mint plant extract;1-furan-3-yl-4-methyl-pentan-1-one;1-(3-Furyl)-4-methyl-1-pentanone;1-(3-Furanyl)-4-methyl-1-pentanone;1-[3]Furyl-4-methyl-pentan-1-on;

Chemical Property of (3-glycidoxypropyl)-1,1,3,3-tetramethyldisiloxane

Chemical Property:

• Refractive Index: 1.4271
• Boiling Point: 92-98°C / 0.2
• PSA: 30.99000
• LogP: 1.99700

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-glycidoxypropyl)-1,1,3,3-tetramethyldisiloxane

There total 2 articles about (3-glycidoxypropyl)-1,1,3,3-tetramethyldisiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.7%

Allyl glycidyl ether (106-92-3,25639-25-2,90907-93-0) + 1,1,3,3-Tetramethyldisiloxane (3277-26-7) → glycidyl 1-propenyl ether (1607-23-4) + 1,3-bis(glycidyloxypropyl)-1,1,3,3-tetramethyldisiloxane (126-80-7) + 1,1,3,3-tetramethyl-1-(3-(oxiran-2-ylmethoxy)propyl)disiloxane (17980-29-9) + 1-(1-methyl-2-glycidoxyethyl)-1,1,3,3-tetramethyldisiloxane (1567764-85-5)

Guidance literature:

With [{SiO₂}O₂Si(Me)(CH₂)3SBu]2PtCl₂; In toluene; at 80 ℃; for 10h; regioselective reaction;

DOI:10.1134/S107036321801005X

Reference yield:

Allyl glycidyl ether (106-92-3,25639-25-2,90907-93-0) + 1,1,3,3-Tetramethyldisiloxane (3277-26-7) → 1,3-bis(glycidyloxypropyl)-1,1,3,3-tetramethyldisiloxane (126-80-7) + 1,1,3,3-tetramethyl-1-(3-(oxiran-2-ylmethoxy)propyl)disiloxane (17980-29-9) + 1-(1-methyl-2-glycidoxyethyl)-1,1,3,3-tetramethyldisiloxane (1567764-85-5)

Guidance literature:

With cis-bis(dibenzyl sulfide)Pt(II) dichloride; In dichloromethane; toluene; at 80 - 100 ℃; Sealed tube;

DOI:10.1134/S1070363214010095

Reference yield: 98.0%

1,1,3,3-tetramethyl-1-(3-(oxiran-2-ylmethoxy)propyl)disiloxane (17980-29-9) + cis-2,3-bis(4-methylbenzensulfonate)-7-oxa-bicyclo-[2.2.1]hept-5-ene-2,3-dimethanol (165727-57-1) → C32H48O10S2Si2

Guidance literature:

With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In dichloromethane; for 72h;

DOI:10.1002/pola.26926

upstream raw materials:

Allyl glycidyl ether

1,1,3,3-Tetramethyldisiloxane