phenylisonitrile(triphenylsilyl)gold(I)

Base Information

Chemical Name:phenylisonitrile(triphenylsilyl)gold(I)
CAS No.:116785-45-6
Molecular Formula:C₂₅H₂₀AuNSi
Molecular Weight:559.493
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylisonitrile(triphenylsilyl)gold(I)

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Technology Process of phenylisonitrile(triphenylsilyl)gold(I)

There total 2 articles about phenylisonitrile(triphenylsilyl)gold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: triphenylsilyl lithium

: 67623-10-3
(phenyl isonitrile)gold(I) chloride

: 116785-45-6
phenylisonitrile(triphenylsilyl)gold(I)

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; To a soln. of PhNCAuCl was added dropwise at 0 °C under exclusion of light LiSiPh3 and the react. was stopped by addn. of dry ice. The volatile was removed under high vac., residue resolved in ether; column chromy. (Al2O3/silica gel 2:1, -10 °C, ether); resolving in petroleum ether at -25 °C, filtration, recrystn. from ether/petroleum ether at -25 °C, drying in high vac.; fast decompn.; detected by NMR;

Reference yield:

: triphenylsilyl lithium

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1197040-29-1,931-54-4
phenyl isocyanate

: 116785-45-6
phenylisonitrile(triphenylsilyl)gold(I)

Guidance literature:: In tetrahydrofuran; byproducts: LiCl, tetrahydrothiophene; To a soln. of THTAuCl was added dropwise at 0 °C under exclusion of light LiSiPh3 and added phenylisonitrile and the react. was stopped by addn. of dry ice. The volatile was removed under high vac., residue resolved in ether; column chromy. (Al2O3/silica gel 2:1, -10 °C, ether); resolving in petroleum ether at -25 °C, filtration, recrystn. from ether/petroleum ether at -25 °C, drying in high vac.; fast decompn.; detected by NMR;