Imidazolidine, 1,3-dihydroxy-4,4,5,5-tetramethyl-2-phenyl-

Base Information

Chemical Name:Imidazolidine, 1,3-dihydroxy-4,4,5,5-tetramethyl-2-phenyl-
CAS No.:18389-99-6
Molecular Formula:C13H20N2O2
Molecular Weight:236.314
Hs Code.:

Synonyms:Imidazolidine,1,3-dihydroxy-4,4,5,5-tetramethyl-2-phenyl;1,3-Dihydroxy-2-phenyl-4,4,5,5-tetramethylimidazolidine;4,4,5,5-tetramethyl-2-phenyl-imidazolidine-1,3-diol;1,3-Dihydroxy-4,4,5,5-tetramethyl-2-phenyl-imidazolidin;1,3-dihydroxyl-2-phenyl-4,4,5,5-tetramethylimidazolidine;1,3-Dihydroxy-2-phenyl-4,4,5,5-tetramethylimidazolin;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Imidazolidine, 1,3-dihydroxy-4,4,5,5-tetramethyl-2-phenyl-

Chemical Property:

Melting Point:168-169 °C
Boiling Point:373.9±42.0 °C(Predicted)
PSA：46.94000
Density:1.148±0.06 g/cm3(Predicted)
LogP:2.51420

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Imidazolidine, 1,3-dihydroxy-4,4,5,5-tetramethyl-2-phenyl-

There total 5 articles about Imidazolidine, 1,3-dihydroxy-4,4,5,5-tetramethyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 14384-45-3
N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

: 100-52-7
benzaldehyde

: 18389-99-6
1,3-dihydroxyl-2-phenyl-4,4,5,5-tetramethylimidazolidine

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2007.07.051

Reference yield: 70.0%

: 351902-03-9
2-Phenyl-4,4,5,5-tetramethylimidazolidine

: 18389-99-6
1,3-dihydroxyl-2-phenyl-4,4,5,5-tetramethylimidazolidine

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 6 ℃; for 0.5h; ice cooling;
DOI:10.1002/1521-3765(20010504)7:9<2007::AID-CHEM2007>3.0.CO;2-7

Reference yield:

: 3964-18-9
2,3-dimethyl-2,3-dinitrobutane

: 18389-99-6
1,3-dihydroxyl-2-phenyl-4,4,5,5-tetramethylimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / Al/Hg / tetrahydrofuran; H₂O / 0.75 h / -7 - -2 °C

2: 96 percent / p-TsOH*H₂O / methanol / 48 h / 20 °C

With aluminum amalgam; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.tet.2007.07.051