Welcome to LookChem.com Sign In|Join Free
  • or

3964-18-9

Post Buying Request

3964-18-9 Suppliers

Recommended suppliersmore

Product FOB Price Min.Order Supply Ability Supplier
2,3-DIMETHYL-2,3-DINITROBUTANE
Cas No: 3964-18-9
USD $ 1.0-3.0 / Gram 1 Gram 4 Metric Ton/Month Chemsigma International Co.,Ltd. Contact Supplier
Factory Supply 2,3-dimethyl-2,3-dinitrobutane
Cas No: 3964-18-9
No Data 1 1 Ality Chemical Corporation Contact Supplier
2,3-Dimethyl-2,3-dinitrobutane
Cas No: 3964-18-9
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
Factory supply 2,3-Dimethyl-2,3-dinitrobutane 3964-18-9 high quality
Cas No: 3964-18-9
No Data No Data Metric Ton/Day Hubei Taiho Chemical Co.,LTD Contact Supplier
High purity 2,3-Dimethyl-2,3-dinitrobutane 98% TOP1 supplier in China
Cas No: 3964-18-9
No Data 100 Gram 1-100 Metric Ton/Day Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
2,3-DIMETHYL-2,3-DINITROBUTANE-
Cas No: 3964-18-9
No Data 1 Kilogram 10 Metric Ton/Month Henan Tianfu Chemical Co., Ltd. Contact Supplier
Low price CAS 3964-18-9 with high-quality service
Cas No: 3964-18-9
USD $ 146.0-176.0 / Gram 10 Gram 1000 Kilogram/Day Zhuozhou Wenxi import and Export Co., Ltd Contact Supplier
whmulei fast delivery 3964-18-9 2,3-DIMETHYL-2,3-DINITROBUTANE china supplier
Cas No: 3964-18-9
USD $ 6.0-12.0 / Gram 50 Gram 100000 Kilogram/Day WUHAN MULEI NEW MATERIAL CO., LTD Contact Supplier
Butane,2,3-dimethyl-2,3-dinitro- 3964-18-9
Cas No: 3964-18-9
No Data 1 Kilogram 10000 Metric Ton/Month Shanghai Upbio Tech Co.,Ltd Contact Supplier
High Purity 2,3-DIMETHYL-2,3-DINITROBUTANE Cas No: 3964-18-9
Cas No: 3964-18-9
USD $ 1.0-3.0 / Gram 10 Gram 1000 Kilogram/Month Wuhan Monad Medicine Tech Co.,LTD Contact Supplier

3964-18-9 Usage

Chemical Properties

white to off-white crystals or cryst. powder

Synthesis Reference(s)

Journal of the American Chemical Society, 96, p. 2580, 1974 DOI: 10.1021/ja00815a043The Journal of Organic Chemistry, 35, p. 295, 1970
InChI:InChI=1/C6H12N2O4/c1-5(2,7(9)10)6(3,4)8(11)12/h1-4H3

3964-18-9 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (156345)  2,3-Dimethyl-2,3-dinitrobutane  98% 3964-18-9 156345-10G 893.88CNY Detail
Aldrich (156345)  2,3-Dimethyl-2,3-dinitrobutane  98% 3964-18-9 156345-50G 3,446.82CNY Detail

3964-18-9SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,3-DIMETHYL-2,3-DINITROBUTANE

1.2 Other means of identification

Product number -
Other names 2,3-dinitro-2,3-dimethylbutane

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:3964-18-9 SDS

3964-18-9Synthetic route

Diethyl ethylsodiomalonate
18995-13-6

Diethyl ethylsodiomalonate

2-nitro-2-thiocyanatopropane
74974-44-0

2-nitro-2-thiocyanatopropane

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

2,3-bis(ethoxycarbonyl)-2,3-diethylsuccinic acid diethyl ester
42798-10-7

2,3-bis(ethoxycarbonyl)-2,3-diethylsuccinic acid diethyl ester

Conditions
ConditionsYield
In dimethyl sulfoxide for 5h; Photolysis;A 95%
B 53%
lithium 2-nitropropane
3958-63-2

lithium 2-nitropropane

diphenyliodonium bromide
1483-73-4

diphenyliodonium bromide

A

formaldehyd
50-00-0

formaldehyd

B

iodobenzene
591-50-4

iodobenzene

C

biphenyl
92-52-4

biphenyl

D

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

E

2-nitro-2-phenylpropane
3457-58-7

2-nitro-2-phenylpropane

F

benzene
71-43-2

benzene

Conditions
ConditionsYield
In methanol at 30℃; for 48h; Mechanism; Product distribution; other diaryliodonium bromides, other times, effect of light and oxygen;A 38%
B 94%
C 5%
D 5%
E 41%
F 43%
2,3-Dihydro-2,2,3,3,5,6-hexamethylpyrazine-1,4-dioxide
14384-47-5

2,3-Dihydro-2,2,3,3,5,6-hexamethylpyrazine-1,4-dioxide

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

dimethylglyoxal
431-03-8

dimethylglyoxal

Conditions
ConditionsYield
With ozone In chloroform-d1 at -78℃; for 0.25h;A 93%
B n/a
1-methyl-1-nitroethyl p-nitrophenyl sulphide
66463-89-6

1-methyl-1-nitroethyl p-nitrophenyl sulphide

2-nitropropane sodium salt

2-nitropropane sodium salt

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 5h; Irradiation;92%
In N,N-dimethyl-formamide for 4h; Product distribution; Irradiation; dark, reaction in the presence of free-radical scavengers; reaction with other α-nitrosulphides;71 % Chromat.
2-nitropropane
79-46-9

2-nitropropane

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
Stage #1: 2-nitropropane With sodium hydroxide for 0.5h; Cooling with ice;
Stage #2: With bromine In ethanol at 90℃; for 2.5h; Cooling with ice;
91.2%
With bromine; sodium hydroxide In ethanol at 84℃; for 3h;83%
Stage #1: 2-nitropropane With bromine; sodium hydroxide In water Cooling with ice;
Stage #2: In ethanol; water at 90℃; for 3h;
81%
2-bromo-2-nitropropane
5447-97-2

2-bromo-2-nitropropane

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
With sodium tert-butyl thiolate In N,N-dimethyl-formamide at 25℃; Irradiation;90%
With 2-mercaptopyridine-1-oxide sodium salt In methanol for 21h;32%
With sodium tert-butyl thiolate In N,N-dimethyl-formamide Product distribution; Irradiation; Products distribution at various temperatures;
lithium 2-nitropropane
3958-63-2

lithium 2-nitropropane

diphenyliodonium bromide
1483-73-4

diphenyliodonium bromide

A

iodobenzene
591-50-4

iodobenzene

B

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

C

2-nitro-2-phenylpropane
3457-58-7

2-nitro-2-phenylpropane

D

benzene
71-43-2

benzene

Conditions
ConditionsYield
With isopropenylbenzene In methanol at 30℃; for 48h; Further byproducts given;A 88%
B 2%
C 67%
D 8%
2-nitropropane sodium salt

2-nitropropane sodium salt

2,2'-dipyrimidyl disulfide
15718-46-4

2,2'-dipyrimidyl disulfide

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-methyl-1-nitroethylpyrimidin-2-yl sulphide
95106-83-5

1-methyl-1-nitroethylpyrimidin-2-yl sulphide

Conditions
ConditionsYield
With oxygen In N,N-dimethyl-formamide for 8h;A 7%
B 86%
2-nitro-2-nitrosopropane
5275-46-7

2-nitro-2-nitrosopropane

A

2,2-dinitropropane
595-49-3

2,2-dinitropropane

B

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

C

acetone
67-64-1

acetone

D

2-Nitro-2-nitrosooxy-propane

2-Nitro-2-nitrosooxy-propane

Conditions
ConditionsYield
In 1,1,2-Trichloro-1,2,2-trifluoroethane at 31℃;A n/a
B n/a
C 83%
D 17%
2-nitropropane
79-46-9

2-nitropropane

6-nitro-N-propyl-2-trichloromethylquinazolin-4-amine
1220564-53-3

6-nitro-N-propyl-2-trichloromethylquinazolin-4-amine

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

2-(1-chloro-2-methylprop-1-enyl)-6-nitro-N-propylquinazolin-4-amine
1220564-57-7

2-(1-chloro-2-methylprop-1-enyl)-6-nitro-N-propylquinazolin-4-amine

Conditions
ConditionsYield
Stage #1: 2-nitropropane With tetra(n-butyl)ammonium hydroxide In dichloromethane; water at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 6-nitro-N-propyl-2-trichloromethylquinazolin-4-amine In dichloromethane; water at 20℃; for 4h; UV-irradiation; Inert atmosphere;
A n/a
B 83%
[bis(acetoxy)iodo]benzene
3240-34-4

[bis(acetoxy)iodo]benzene

2-isocyano-5-methyl-1,1'-biphenyl
1428264-89-4

2-isocyano-5-methyl-1,1'-biphenyl

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

2,6-dimethylphenanthridine
1402547-38-9

2,6-dimethylphenanthridine

Conditions
ConditionsYield
With 2-nitropropane; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 2h; Reagent/catalyst; Solvent; Inert atmosphere; Green chemistry;A 51%
B 82%
lithium 2-nitropropane
3958-63-2

lithium 2-nitropropane

bronidox
30007-47-7

bronidox

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

5-nitro-5-(2-nitro-1-methylethyl)-1,3-dioxane
91173-72-7

5-nitro-5-(2-nitro-1-methylethyl)-1,3-dioxane

C

5-nitro-5-(5-nitro-1,3-dioxa-5-cyclohexyl)-1,3-dioxacyclohexane
86251-74-3

5-nitro-5-(5-nitro-1,3-dioxa-5-cyclohexyl)-1,3-dioxacyclohexane

D

LiBr

LiBr

Conditions
ConditionsYield
In dimethyl sulfoxide at 20℃; for 3h;A n/a
B 80%
C 15%
D n/a
In dimethyl sulfoxide at 20℃; for 3h; Yields of byproduct given;A 40%
B n/a
C n/a
D n/a
1-methyl-1-nitroethyl p-nitrophenyl sulphide
66463-89-6

1-methyl-1-nitroethyl p-nitrophenyl sulphide

nitrocyclohexane sodium salt

nitrocyclohexane sodium salt

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-(1-methyl-1-nitroethyl)-1-nitrocyclohexane
1636-28-8

1-(1-methyl-1-nitroethyl)-1-nitrocyclohexane

Conditions
ConditionsYield
In dimethyl sulfoxide for 4h; Irradiation;A 14%
B 76%
2-nitro-propan-2-ide
20846-00-8

2-nitro-propan-2-ide

2-nitro-2-thiocyanatopropane
74974-44-0

2-nitro-2-thiocyanatopropane

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
In dimethyl sulfoxide for 2h; Irradiation;72%
Mechanism; Irradiation; reactions with further anions in various conditions;
2-nitro-propan-2-ide
20846-00-8

2-nitro-propan-2-ide

1-(dichloromethyl)-5-nitroisoquinoline

1-(dichloromethyl)-5-nitroisoquinoline

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-(2-methyl-1-propenyl)-5-nitroisoquinoline

1-(2-methyl-1-propenyl)-5-nitroisoquinoline

C

1-(1-Chloro-2-methyl-propenyl)-5-nitro-isoquinoline

1-(1-Chloro-2-methyl-propenyl)-5-nitro-isoquinoline

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 24h; Irradiation;A n/a
B 72%
C n/a
In dichloromethane; water for 24h; Product distribution; Irradiation; with different scavengers and solvent;A n/a
B 38%
C 30%
In dichloromethane; water for 24h; Irradiation;A n/a
B 38%
C 30%
sodium 2-nitropropane
24163-39-1

sodium 2-nitropropane

2-nitro-2-thiocyanatopropane
74974-44-0

2-nitro-2-thiocyanatopropane

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
In dimethyl sulfoxide for 2h; Photolysis;72%
lithium 2-nitropropane
3958-63-2

lithium 2-nitropropane

2,4-dibromo-2,4-dinitropentane

2,4-dibromo-2,4-dinitropentane

A

2-bromo-2-nitropropane
5447-97-2

2-bromo-2-nitropropane

B

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

C

trans-1,2-dimethyl-1,2-dinitrocyclopropane

trans-1,2-dimethyl-1,2-dinitrocyclopropane

Conditions
ConditionsYield
In dimethyl sulfoxide at 18 - 20℃; for 0.00833333h;A 5%
B 70%
C 25%
With m-DNB In dimethyl sulfoxide at 18 - 20℃; for 0.00833333h;A 25%
B 5%
C 20%
2,2-dinitropropane
595-49-3

2,2-dinitropropane

sodium p-chlorothiophenolate
18803-44-6

sodium p-chlorothiophenolate

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-methyl-1-nitroethyl p-chlorophenyl sulphide
52755-34-7

1-methyl-1-nitroethyl p-chlorophenyl sulphide

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 18h; Photolysis;A n/a
B 69%
tetramethyl succinic acid
630-51-3

tetramethyl succinic acid

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
With nitronium tetrafluoborate; silver carbonate In N,N-dimethyl acetamide at 90℃; for 12h; Inert atmosphere; Schlenk technique; regioselective reaction;69%
2-bromo-2-methyl-propionitrile
41658-69-9

2-bromo-2-methyl-propionitrile

2-nitropropane
79-46-9

2-nitropropane

A

α,α-dimethyl-β-nitroisovaleronitrile
29770-62-5

α,α-dimethyl-β-nitroisovaleronitrile

B

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

Conditions
ConditionsYield
With potassium tert-butylate In N,N,N,N,N,N-hexamethylphosphoric triamideA 68%
B n/a
6-nitro-2-trichloromethylquinazolin-4(3H)-one
98591-28-7

6-nitro-2-trichloromethylquinazolin-4(3H)-one

2-lithio-2-nitropropane
147225-22-7

2-lithio-2-nitropropane

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

2-(1-chloro-2-methylprop-1-enyl)-6-nitroquinazolin-4(3H)-one
1220564-78-2

2-(1-chloro-2-methylprop-1-enyl)-6-nitroquinazolin-4(3H)-one

Conditions
ConditionsYield
In dimethyl sulfoxide at 20℃; for 2h; UV-irradiation; Inert atmosphere;A n/a
B 67%
2-bromo-2-nitropropane
5447-97-2

2-bromo-2-nitropropane

4(5)-nitroimidazole anion
36954-04-8

4(5)-nitroimidazole anion

A

2,2-dinitropropane
595-49-3

2,2-dinitropropane

B

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

C

1-(1-methyl-1-nitroethyl)-4-nitroimidazole
117836-30-3

1-(1-methyl-1-nitroethyl)-4-nitroimidazole

Conditions
ConditionsYield
With sodium persulfate; potassium hexacyanoferrate(III) for 1h;A n/a
B 20%
C 63%
lithium 2-nitropropane
3958-63-2

lithium 2-nitropropane

2-chloro-2-nitrohept-6-ene
96246-33-2

2-chloro-2-nitrohept-6-ene

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

2,3-dimethyl-2,3-dinitro-7-octene
96246-38-7

2,3-dimethyl-2,3-dinitro-7-octene

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 48h; Irradiation;A 12%
B 63%
2-nitro-propan-2-ide
20846-00-8

2-nitro-propan-2-ide

1-nitro-1-thiocyanatocyclohexane
74974-48-4

1-nitro-1-thiocyanatocyclohexane

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-(1-methyl-1-nitroethyl)-1-nitrocyclohexane
1636-28-8

1-(1-methyl-1-nitroethyl)-1-nitrocyclohexane

Conditions
ConditionsYield
In dimethyl sulfoxide for 4h; Irradiation;A 16%
B 61%
1-methyl-1-nitroethyl p-nitrophenyl sulphide
66463-89-6

1-methyl-1-nitroethyl p-nitrophenyl sulphide

diethyl ethylmalonate sodium salt
18995-13-6

diethyl ethylmalonate sodium salt

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

diethyl 2-(1-nitro-1-methylethyl)-2-ethylmalonate
75376-77-1

diethyl 2-(1-nitro-1-methylethyl)-2-ethylmalonate

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 4h; Irradiation;A 61%
B 21%
sodium 2-nitropropane
24163-39-1

sodium 2-nitropropane

1-nitro-1-thiocyanatocyclohexane
74974-48-4

1-nitro-1-thiocyanatocyclohexane

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-(1-methyl-1-nitroethyl)-1-nitrocyclohexane
1636-28-8

1-(1-methyl-1-nitroethyl)-1-nitrocyclohexane

Conditions
ConditionsYield
In dimethyl sulfoxide for 5h; Photolysis;A 30%
B 60%
α-nitroisopropyl phenyl sulfone
41774-06-5

α-nitroisopropyl phenyl sulfone

sodium p-chlorothiophenolate
18803-44-6

sodium p-chlorothiophenolate

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1-methyl-1-nitroethyl p-chlorophenyl sulphide
52755-34-7

1-methyl-1-nitroethyl p-chlorophenyl sulphide

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 4h; Photolysis;A n/a
B 59%
di(benzothiazol-2-yl)disulfide
120-78-5

di(benzothiazol-2-yl)disulfide

2-nitropropane sodium salt

2-nitropropane sodium salt

A

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

B

1,3-benzothiazol-2-yl 1-methyl-1-nitroethyl sulphide
75376-74-8

1,3-benzothiazol-2-yl 1-methyl-1-nitroethyl sulphide

Conditions
ConditionsYield
With oxygen In N,N-dimethyl-formamide for 8h;A 11%
B 58%
2-nitro-2-nitrosopropane
5275-46-7

2-nitro-2-nitrosopropane

bis(trifluoroacetyl)peroxide
383-73-3

bis(trifluoroacetyl)peroxide

A

2,2-dinitropropane
595-49-3

2,2-dinitropropane

B

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

C

acetone
67-64-1

acetone

D

2-Nitro-2-nitrosooxy-propane

2-Nitro-2-nitrosooxy-propane

E

1,1,1-Trifluoro-2-methyl-2-nitro-propane

1,1,1-Trifluoro-2-methyl-2-nitro-propane

Conditions
ConditionsYield
In 1,1,2-Trichloro-1,2,2-trifluoroethane at 31℃; Rate constant; Mechanism; Product distribution; var. ratio diacyl peroxide;A 55%
B n/a
C 30%
D 7%
E 8%
lithium 2-nitropropane
3958-63-2

lithium 2-nitropropane

(p-methylphenyl)phenyliodonium bromide
2665-60-3

(p-methylphenyl)phenyliodonium bromide

A

formaldehyd
50-00-0

formaldehyd

B

iodobenzene
591-50-4

iodobenzene

C

2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

D

4-tolyl iodide
624-31-7

4-tolyl iodide

Conditions
ConditionsYield
In methanol at 30℃; for 48h; Further byproducts given;A 37%
B 44%
C 6%
D 54%
2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

2,3-dimethyl-2,3-diaminobutane
20485-44-3

2,3-dimethyl-2,3-diaminobutane

Conditions
ConditionsYield
With hydrogenchloride; tin for 3h; Heating;81%
With hydrogenchloride; tin75%
With hydrogenchloride; tin In water at 105℃; for 4h;60%
2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine
14384-45-3

N,N'-dihydroxy-2,3-dimethylbutane-2,3-diamine

Conditions
ConditionsYield
With aluminum amalgam In tetrahydrofuran; water at -7 - -2℃; for 0.75h;79%
With aluminum amalgam In tetrahydrofuran; water at 0℃; for 0.333333h;76%
With ammonium chloride; zinc In tetrahydrofuran at 4 - 6℃; for 16.5h;68%
2,3-dimethyl-2,3-dinitrobutane
3964-18-9

2,3-dimethyl-2,3-dinitrobutane

2,3-diamino-2,3-dimethylbutane bishydrochloride
75804-28-3

2,3-diamino-2,3-dimethylbutane bishydrochloride

Conditions
ConditionsYield
Stage #1: 2,3-dimethyl-2,3-dinitrobutane With hydrogenchloride; tin In water at 50℃; for 2h; Reflux;
Stage #2: With potassium hydroxide In water
61%
Stage #1: 2,3-dimethyl-2,3-dinitrobutane With hydrogenchloride; tin In water at 50℃; for 2.16667h; Reflux;
Stage #2: With potassium hydroxide In water
Stage #3: With hydrogenchloride In water pH=2;
61%

Please post your buying leads,so that our qualified suppliers will soon contact you!

*Required Fields