2-Naphthalenol, 1-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-

Base Information

Chemical Name:2-Naphthalenol, 1-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-
CAS No.:187605-87-4
Molecular Formula:C23H25NO
Molecular Weight:331.458
Hs Code.:

Synonyms:

Suppliers and Price of 2-Naphthalenol, 1-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Naphthalenol, 1-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2-Naphthalenol, 1-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-

There total 1 articles about 2-Naphthalenol, 1-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 708-06-5
2-hydroxynaphthalene-1-carbaldehyde

: 187605-87-4,937030-19-8
1-[[(2,6-diisopropylphenyl)imino]methylenyl]-2-naphthalenol

Guidance literature:: With acetic acid; In methanol; at 60 ℃; for 4h;

Reference yield: 98.5%

: (N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II)

: 187605-87-4,937030-19-8
1-[[(2,6-diisopropylphenyl)imino]methylenyl]-2-naphthalenol

: 53597-69-6
(1,3,5-triaza-7-phosphaadamantane)

: 630416-12-5
Pd(CH₃)PN₃(CH₂)6C₆H₃(CH(CH₃)2)2NCHC₆H₂O(CH)4

Guidance literature:: In methanol; toluene; ligand in MeOH was introduced into Schlenk flask with Pd-complex in toluene at -30°C, second ligand in toluene was slowly added, stirred for 30 min under Ar, warmed to room temp., stirred overnight; solvent was removed in vacuo, cooled to -78°C, pentane was added,filtered, washed with pentane at -78°C; elem. anal.;
DOI:10.1021/ic0341284

Reference yield: 84.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 187605-87-4,937030-19-8
1-[[(2,6-diisopropylphenyl)imino]methylenyl]-2-naphthalenol

: 1030937-83-7
(1,5-cyclooctadiene)(1-[(2,6-diisopropylphenyl)iminomethylenyl]-2-naphthalenolato)iridium(I)

Guidance literature:: With sodium hydride; In tetrahydrofuran; byproducts: H2, NaCl; NaH added to THF soln. of ligand; stirred at room temp. for 2 h; soln. of Ir complex in THF added; stirred at room temp. for 2 h; solvent evapd. in vac.; dissolved in CH2Cl2; filtered over Na2SO4; solvent removed from filtrate in vac.; washed with pentane; dried in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2008.02.003