Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis-

Base Information

Chemical Name:Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis-
CAS No.:1889-01-6
Molecular Formula:C10H8Cl2O4
Molecular Weight:263.077
Hs Code.:
DSSTox Substance ID:DTXSID90445466
Nikkaji Number:J1.341.560I

Synonyms:Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis-;1889-01-6;SCHEMBL2117441;DTXSID90445466;1,4-phenylenedioxy diacetyl chloride;p-Phenylenedioxybis(acetic acid chloride)

Suppliers and Price of Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis-

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:261.9799641
Heavy Atom Count:16
Complexity:223

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1OCC(=O)Cl)OCC(=O)Cl

Technology Process of Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis-

There total 8 articles about Acetyl chloride, 2,2'-[1,4-phenylenebis(oxy)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 2245-53-6
2,2'-[1,4-phenylenebis(oxy)]bisacetic acid

: 1889-01-6
(1,4-phenylenedioxy)di(acetyl chloride)

Guidance literature:: With thionyl chloride; N-benzyl-N,N,N-triethylammonium chloride; In chloroform; for 4h; Heating;
DOI:10.1080/00397919608003507

Reference yield:

: 5897-78-9
(4-ethoxycarbonylmethoxy-phenoxy)-acetic acid ethyl ester

: 1889-01-6
(1,4-phenylenedioxy)di(acetyl chloride)

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 1.) aq. NaOH, 2.) aq. HCl / 4 h / Heating

2: (COCl)2, DMF / benzene / 21 h / 50 °C

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In benzene;

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1889-01-6
(1,4-phenylenedioxy)di(acetyl chloride)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) K₂CO₃ / 1.) CH₃CN, 50 deg C, 30 min, 2.) CH₃CN, reflux, 6 h

2: 94 percent / 1.) aq. NaOH, 2.) aq. HCl / 4 h / Heating

3: (COCl)2, DMF / benzene / 21 h / 50 °C

With hydrogenchloride; sodium hydroxide; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In benzene;