N-Boc-D-valine N'-methoxy-N'-methylamide

Base Information

Chemical Name:N-Boc-D-valine N'-methoxy-N'-methylamide
CAS No.:190260-92-5
Molecular Formula:C12H24N2O4
Molecular Weight:260.334
Hs Code.:
Mol file:190260-92-5.mol

Synonyms:(R)-tert-butyl 1-(methoxy(methyl)amino)-3-methyl-1-oxobutan-2-yl carbamate;(R)-N'-methyl-N'-methoxy 2-N-(t-butoxycarbonyl)amino-3-methylbutanamide;N-t-butoxycarbonyl-N'-methoxy-N'-methyl-D-valine amide;N2-{[(1,1-dimethylethyl)oxy]carbonyl}-N1-methyl-N1-(methyloxy)valinamide;B-1790;N-Boc-D-valineN'-methoxy-N'-methylamide;

Suppliers and Price of N-Boc-D-valine N'-methoxy-N'-methylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
N-Boc-D-valineN'-methoxy-N'-methylamide 97%
5g
$ 146.67

Total 6 raw suppliers

Chemical Property of N-Boc-D-valine N'-methoxy-N'-methylamide

Chemical Property:

PSA：71.36000
Density:1.039
LogP:1.75990

Purity/Quality:

97% ^*data from raw suppliers

N-Boc-D-valineN'-methoxy-N'-methylamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-Boc-D-valine N'-methoxy-N'-methylamide

There total 5 articles about N-Boc-D-valine N'-methoxy-N'-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 22838-58-0
Boc-D-Val-OH

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 190260-92-5
(R)-tert-butyl (1-(methoxy(methyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: Boc-D-Val-OH; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 0.5h;

N,O-dimethylhydroxylamine*hydrochloride; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 14h;
DOI:10.1021/jo402670d

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 190260-92-5
(R)-tert-butyl (1-(methoxy(methyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 22838-58-0
Boc-D-Val-OH

: 16645-06-0
N,N-dimethylhydroxylamine hydrochloride

: 190260-92-5
(R)-tert-butyl (1-(methoxy(methyl)amino)-3-methyl-1-oxobutan-2-yl)carbamate

Guidance literature:: Boc-D-Val-OH; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 - 9 ℃; for 0.266667h;

N,N-dimethylhydroxylamine hydrochloride; In tetrahydrofuran; at 9 - 23 ℃; for 1.08333h;