3,6-bis-phenylacetyl-carbazole

Base Information

• Chemical Name: 3,6-bis-phenylacetyl-carbazole
• CAS No.: 700863-22-5
• Molecular Formula: C₂₈H₂₁NO₂
• Molecular Weight: 403.48
• Mol file: 700863-22-5.mol

Synonyms:

Chemical Property of 3,6-bis-phenylacetyl-carbazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,6-bis-phenylacetyl-carbazole

There total 3 articles about 3,6-bis-phenylacetyl-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-carbazolyl-2-phenylacetamide (115552-48-2) → 3,6-bis-phenylacetyl-carbazole (700863-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aluminium chloride; nitrobenzene / 120 °C

2: aluminium chloride; benzene

With aluminium trichloride; nitrobenzene; benzene;

DOI:10.1039/jr9540001341

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 3,6-bis-phenylacetyl-carbazole (700863-22-5)

Guidance literature:

Multi-step reaction with 3 steps

1: methyl magnesium chloride; diethyl ether / anschliessenden Erwaermen mit Phenylacetylchlorid

2: aluminium chloride; nitrobenzene / 120 °C

3: aluminium chloride; benzene

With aluminium trichloride; diethyl ether; methylmagnesium chloride; nitrobenzene; benzene;

DOI:10.1039/jr9540001341

Reference yield:

1-carbazol-3-yl-2-phenyl-ethanone (412023-11-1) + phenylacetyl chloride (103-80-0) → 3,6-bis-phenylacetyl-carbazole (700863-22-5)

Guidance literature:

With aluminium trichloride; benzene;

DOI:10.1039/jr9540001341

upstream raw materials:

1-carbazol-3-yl-2-phenyl-ethanone

phenylacetyl chloride

N-carbazolyl-2-phenylacetamide

9H-carbazole