2-Azetidinone, 4-(4-methoxyphenyl)-1-phenyl-

Base Information

• Chemical Name: 2-Azetidinone, 4-(4-methoxyphenyl)-1-phenyl-
• CAS No.: 19340-69-3
• Molecular Formula: C16H15NO2
• Molecular Weight: 253.301
• DSSTox Substance ID: DTXSID60459878
• Nikkaji Number: J1.822.551D

Synonyms:2-Azetidinone, 4-(4-methoxyphenyl)-1-phenyl-;19340-69-3;SCHEMBL1997854;DTXSID60459878

Chemical Property of 2-Azetidinone, 4-(4-methoxyphenyl)-1-phenyl-

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 253.110278721
• Heavy Atom Count: 19
• Complexity: 317

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C2CC(=O)N2C3=CC=CC=C3

Technology Process of 2-Azetidinone, 4-(4-methoxyphenyl)-1-phenyl-

There total 12 articles about 2-Azetidinone, 4-(4-methoxyphenyl)-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C18H17NO3S2 → 4-(4-methoxy-phenyl)-1-phenyl-azetidin-2-one (19340-69-3)

Guidance literature:

With trimethylborane; In water; toluene; at 80 ℃; for 8h; Microwave irradiation;

Reference yield: 67.0%

ethyl bromoacetate (105-36-2) + N-(4-methoxybenzylidene)aniline (1613-96-3) → 4-(4-methoxy-phenyl)-1-phenyl-azetidin-2-one (19340-69-3)

Guidance literature:

With diethylzinc; RhCl(PPh₃)3; In hexane; toluene; at 40 ℃; for 0.5h;

DOI:10.3987/com-02-s(m)10

Reference yield:

(Z)-1-(4-methoxyphenyl)-N-phenylmethanimine (40339-47-7) + bromo(2-ethoxy-2-oxoethyl)zinc (5764-82-9) → 4-(4-methoxy-phenyl)-1-phenyl-azetidin-2-one (19340-69-3)

Guidance literature:

In tetrahydrofuran;

DOI:10.1016/0960-894X(96)00365-4

upstream raw materials:

N-(4-methoxybenzylidene)aniline oxide

tert.-butyl lithium

phenylthioethylene

(Z)-1-(4-methoxyphenyl)-N-phenylmethanimine

Downstream raw materials:

3(R)-(1(R)-hydroxy-3-phenylpropyl)-4(S)-(4-methoxyphenyl)-1-phenyl-2-azetidinone

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