2-Acetamido-5-methoxy-4-nitrobenzoic Acid

Base Information

Chemical Name:2-Acetamido-5-methoxy-4-nitrobenzoic Acid
CAS No.:196194-98-6
Molecular Formula:C10H10N2O6
Molecular Weight:254.199
Hs Code.:2924299090
Mol file:196194-98-6.mol

Synonyms:2-ACETAMIDO-5-METHOXY-4-NITROBENZOIC ACID;4-Nitro-6-acetamino-3-methoxy-benzoesaeure;2-acetylamino-5-methoxy-4-nitro-benzoic acid;2-Acetylamino-5-methoxy-4-nitro-benzoesaeure;

Suppliers and Price of 2-Acetamido-5-methoxy-4-nitrobenzoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Acetamido-5-methoxy-4-nitrobenzoicacid
250mg
$ 165.00

Crysdot
2-Acetamido-5-methoxy-4-nitrobenzoicacid 97%
5g
$ 342.00

American Custom Chemicals Corporation
2-ACETAMIDO-5-METHOXY-4-NITROBENZOIC ACID 95.00%
5MG
$ 505.03

Alichem
2-Acetamido-5-methoxy-4-nitrobenzoicacid
5g
$ 633.36

Alichem
2-Acetamido-5-methoxy-4-nitrobenzoicacid
1g
$ 213.15

AK Scientific
2-Acetamido-5-methoxy-4-nitrobenzoicacid
1g
$ 228.00

Total 13 raw suppliers

Chemical Property of 2-Acetamido-5-methoxy-4-nitrobenzoic Acid

Chemical Property:

Vapor Pressure:6.59E-12mmHg at 25°C
Boiling Point:526.4oC at 760 mmHg
Flash Point:272.1oC
PSA：121.45000
Density:1.487g/cm3
LogP:1.85620

Purity/Quality:

97% ^*data from raw suppliers

2-Acetamido-5-methoxy-4-nitrobenzoicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Acetamido-5-methoxy-4-nitrobenzoic Acid

There total 3 articles about 2-Acetamido-5-methoxy-4-nitrobenzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.7%

: 196194-97-5
N-(4-methoxy-2-methyl-5-nitrophenyl)acetamide

: 196194-98-6
2-acetamido-5-methoxy-4-nitrobenzoic acid

Guidance literature:: With potassium permanganate; water; magnesium sulfate; at 80 ℃; for 1.75h;

Reference yield: 54.0%

: 196194-97-5
N-(4-methoxy-2-methyl-5-nitrophenyl)acetamide

: 7487-88-9
magnesium sulfate

: 196194-98-6
2-acetamido-5-methoxy-4-nitrobenzoic acid

Guidance literature:: With potassium permanganate; In water;

Reference yield:

: 102-50-1
2-methyl-4-methoxyaniline

: 196194-98-6
2-acetamido-5-methoxy-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C / Inert atmosphere

2: trifluoroacetic acid; sodium nitrite / 0 - 20 °C / Inert atmosphere

3: potassium permanganate; magnesium sulfate / water / 1.5 h / 80 °C / Inert atmosphere

With pyridine; potassium permanganate; magnesium sulfate; trifluoroacetic acid; sodium nitrite; In water;
DOI:10.1016/j.tet.2011.11.010