2-Fluoro-1-nitro-4-vinyl-benzene

Base Information

Chemical Name:2-Fluoro-1-nitro-4-vinyl-benzene
CAS No.:197777-90-5
Molecular Formula:C8H6FNO2
Molecular Weight:167.14
Hs Code.:
European Community (EC) Number:820-538-7
DSSTox Substance ID:DTXSID70472770
Wikidata:Q82301905

Synonyms:197777-90-5;2-Fluoro-1-nitro-4-vinyl-benzene;4-ethenyl-2-fluoro-1-nitrobenzene;Benzene, 4-ethenyl-2-fluoro-1-nitro-;2-Fluoro-1-nitro-4-vinylbenzene;4-vinyl-2-fluoronitrobenzene;SCHEMBL1546955;DTXSID70472770;OKNXGWILKMLMGV-UHFFFAOYSA-N;ZB0633;EN300-117026

Suppliers and Price of 2-Fluoro-1-nitro-4-vinyl-benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Fluoro-1-nitro-4-vinyl-benzene

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:167.03825660
Heavy Atom Count:12
Complexity:190

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CC1=CC(=C(C=C1)[N+](=O)[O-])F

Technology Process of 2-Fluoro-1-nitro-4-vinyl-benzene

There total 4 articles about 2-Fluoro-1-nitro-4-vinyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 321-23-3
4-bromo-2-fluoronitrobenzene

: 7486-35-3
tri-n-butyl(vinyl)tin

: 197777-90-5
3-fluoro-4-nitrostyrene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine; In toluene; for 5h; Heating / reflux;

Reference yield: 60.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: (3-Fluoro-4-nitro-benzyl)-triphenyl-phosphonium; bromide

: 197777-90-5
3-fluoro-4-nitrostyrene

Guidance literature:: With sodium carbonate; In chloroform; water; for 1h; Ambient temperature;
DOI:10.1016/S0040-4039(97)01749-8

Reference yield:

: 446-34-4
2-fluoro-4-methyl-1-nitrobenzene

: 197777-90-5
3-fluoro-4-nitrostyrene

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / NBS, AIBN / CCl₄ / 8 h / Irradiation

2: 100 percent / benzene / 26 h / Ambient temperature

3: 60 percent / Na₂CO₃ / H₂O; CHCl₃ / 1 h / Ambient temperature

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium carbonate; In tetrachloromethane; chloroform; water; benzene;
DOI:10.1016/S0040-4039(97)01749-8