dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane

Base Information

Chemical Name:dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane
CAS No.:79146-05-7
Molecular Formula:C₃₀H₃₀BFO₄S₂
Molecular Weight:548.507
Hs Code.:

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Chemical Property of dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane

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Technology Process of dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane

There total 2 articles about dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79146-03-5
4-dimesitylborylbenzenediazonium chloride

: 2489-52-3
3-(fluorosulfonyl)benzenesulfonyl chloride

: 79146-05-7
dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane

Guidance literature:: In methanol; water; p-(dimesitylboryl)benzenediazonium chloride soln. (prepd. in water/methanol at 0°C) added to 3-fluorosulfonylbenzenesulfonyl chloride/methanol soln.; warmed to room temp.; filtered; washed with water; chromy. (silica gel); characterized IR, NMR, mass spect.;
DOI:10.1016/S0022-328X(00)83994-7

Reference yield:

: 79146-04-6
3-[N-phenylsulfamido]benzenesulfonyl fluoride

: 79146-03-5
4-dimesitylborylbenzenediazonium chloride

: 79146-05-7
dimesityl-4-(3-fluorosulfonylphenylsulfonyl)phenyl borane

Guidance literature:: In methanol; water; byproducts: tris(dimesitylborylphenyl)amine, p-aminophenyldimesitylborane; p-(dimesitylboryl)benzenediazonium chloride soln. (prepd. in water/methanol at 0°C) added to 3-(N-phenylsulfamido)benzenesulfonyl fluoride; extd. with toluene and water; toluene soln. dried; evapd.; chromd. (silica gel), first zone;
DOI:10.1016/S0022-328X(00)83994-7