4-dimesitylborylbenzenediazonium chloride

Base Information

Chemical Name:4-dimesitylborylbenzenediazonium chloride
CAS No.:79146-03-5
Molecular Formula:C₂₄H₂₆BN₂*Cl
Molecular Weight:388.748
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-dimesitylborylbenzenediazonium chloride

Chemical Property:

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Technology Process of 4-dimesitylborylbenzenediazonium chloride

There total 2 articles about 4-dimesitylborylbenzenediazonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79146-02-4
4-(dimesitylboryl)benzenamine

: 110-46-3
isopentyl nitrite

: 79146-03-5
4-dimesitylborylbenzenediazonium chloride

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; treating p-aminophenyldimesitylborane in THF with gaseous HCl; cooling to 0°C; isopentyl nitrite addn.; 10 min;
DOI:10.1016/S0022-328X(00)83994-7

Reference yield:

: 4-aminophenyldimesitylborane hydrochloride

: 110-46-3
isopentyl nitrite

: 79146-03-5
4-dimesitylborylbenzenediazonium chloride

Guidance literature:: In methanol; water; B-compound was reacted with isopentyl nitrite in a mixt. of H2O/MeOH at0°C for 30 min;
DOI:10.1016/S0022-328X(00)81948-8

Reference yield: 40.0%

: 79146-03-5
4-dimesitylborylbenzenediazonium chloride

: 90-15-3
α-naphthol

: 79146-10-4
4-(4-dimesitylborylphenylazo)-1-naphthol

Guidance literature:: With sodium acetate; In tetrahydrofuran; water; p-aminophenyldimesitylborane/THF soln. slowly addn. to chilled THF/watersoln. of 1-naphthol and excess sodium acetate; 2 h at 0°C;
DOI:10.1016/S0022-328X(00)83994-7