[Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF₆

Base Information

Chemical Name:[Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF₆
CAS No.:869780-71-2
Molecular Formula:C₂N₃*C₂₇H₂₉N₅*F₆P*Fe
Molecular Weight:690.414
Hs Code.:

[Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF<sub>6</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF₆

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Technology Process of [Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF₆

There total 1 articles about [Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: ammonium hexafluorophosphate

: iron(II) tetrafluoroborate hexahydrate

: 34723-47-2
potassium dicyanamide

: 316381-49-4
N¹-benzyl-N¹,N²,N²-tris(pyridine-2-ylmethyl)ethane-1,2-diamine

: 869780-71-2
[Fe(II)(N-benzyl-N,N',N'-tris(2-methylpyridyl)ethylenediamine)(N(CN)2)]PF₆

Guidance literature:: In methanol; byproducts: NH4BF4; under Ar; soln. of Fe(BF4)2*6H2O in MeOH added dropwise to soln. of ligand in MeOH; MeOH soln. of KN(CN)2 (excess) added; stirred for 20 min; soln. of NH4PF6 in MeOH added very slowly; filtered; crystd. from filtrate by slow evapn. under Ar for ca. 36 h;
DOI:10.1021/ic0620743