Benzenesulfonamide, 2,2'-diselenobis[N-methyl-

Base Information

Chemical Name:Benzenesulfonamide, 2,2'-diselenobis[N-methyl-
CAS No.:199605-34-0
Molecular Formula:C14H16N2O4S2Se2
Molecular Weight:498.344
Hs Code.:
DSSTox Substance ID:DTXSID90441625
Nikkaji Number:J912.923E
Wikidata:Q82258472

Synonyms:Benzenesulfonamide, 2,2'-diselenobis[N-methyl-;199605-34-0;DTXSID90441625;2,2'-Diselenobis(N-methylbenzenesulfonamide)

Suppliers and Price of Benzenesulfonamide, 2,2'-diselenobis[N-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzenesulfonamide, 2,2'-diselenobis[N-methyl-

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:499.88819
Heavy Atom Count:24
Complexity:547

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNS(=O)(=O)C1=CC=CC=C1[Se][Se]C2=CC=CC=C2S(=O)(=O)NC

Technology Process of Benzenesulfonamide, 2,2'-diselenobis[N-methyl-

There total 6 articles about Benzenesulfonamide, 2,2'-diselenobis[N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 74-89-5
methylamine

: 199605-41-9
bis(2-chlorosulfonylphenyl)diselenide

: 199605-34-0
2,2'-diselenobis(N-methylbenzenesulfonamide)

Guidance literature:: In methanol; acetonitrile; at -10 - 25 ℃; for 3h;
DOI:10.1080/00397919708005450

Reference yield: 67.0%

: 74-89-5
methylamine

: 199605-42-0
2-(bromoseleno)benzenesulfonyl chloride

: 199605-34-0
2,2'-diselenobis(N-methylbenzenesulfonamide)

Guidance literature:: In dichloromethane; at -15 - 20 ℃;

Reference yield:

: 88-21-1
2-amino-1-benzenesulfonic acid

: 199605-34-0
2,2'-diselenobis(N-methylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / NaNO₂, Na₂CO₃, H₂SO₄ / H₂O / 0.5 h / -10 °C

2: 78 percent / H₂O / 4 h / 0 °C

3: 90 percent / PCl₅ / 1.) 150 deg C, 1 h, 2.) C₆H₆, reflux, 3 h

5: 74 percent / acetonitrile; methanol / 3 h / -10 - 25 °C

With phosphorus pentachloride; sulfuric acid; sodium carbonate; sodium nitrite; In methanol; water; acetonitrile;
DOI:10.1080/00397919708005450