Acetic acid, (3-pentadecylphenoxy)-, ethyl ester

Base Information

• Chemical Name: Acetic acid, (3-pentadecylphenoxy)-, ethyl ester
• CAS No.: 200133-85-3
• Molecular Formula: C25H42O3
• Molecular Weight: 390.607
• Mol file: 200133-85-3.mol

Synonyms:

Chemical Property of Acetic acid, (3-pentadecylphenoxy)-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Acetic acid, (3-pentadecylphenoxy)-, ethyl ester

There total 2 articles about Acetic acid, (3-pentadecylphenoxy)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

3-n-Pentadecylphenol (501-24-6) + chloroacetic acid ethyl ester (105-39-5) → ethyl-2-(3-pentadecylphenoxy)acetate (200133-85-3)

Guidance literature:

With potassium carbonate; In acetone; for 24h; Reflux;

DOI:10.3184/174751917X14925986241061

Reference yield:

3-[(Z)-8-pentadecenyl]phenol (501-26-8) → ethyl-2-(3-pentadecylphenoxy)acetate (200133-85-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 20 °C / 3102.97 Torr

2.1: potassium carbonate / acetone / 0.33 h

2.2: 24 h / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethanol; acetone;

DOI:10.1021/acs.jmedchem.1c01542

Reference yield: 90.0%

ethyl-2-(3-pentadecylphenoxy)acetate (200133-85-3) → 3-Pentadecylphenoxyacetic acid (14103-68-5)

Guidance literature:

With Aliquat 336; lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 4h;

DOI:10.1021/acs.jmedchem.1c01542

upstream raw materials:

3-n-Pentadecylphenol

chloroacetic acid ethyl ester

3-[(Z)-8-pentadecenyl]phenol

Downstream raw materials:

3-Pentadecylphenoxyacetic acid

3-Pentadecylphenoxyacetic acid hydrazid

Refernces

• 1、 Sahin, Cigdem,Magomedova, Lilia,Ferreira, Thais A. M.,Liu, Jiabao,Tiefenbach, Jens,Alves, Priscilla S.,Queiroz, Fellipe J. G.,Oliveira, Andressa S. De,Bhattacharyya, Mousumi,Grouleff, Julie,Nogueira, Patrícia C. N.,Silveira, Edilberto R.,Moreira, Daniel C.,Leite, José Roberto Souza De Almeida,Brand, Guilherme D.,Uehling, David,Poda, Gennady,Krause, Henry,Cummins, Carolyn L.,Romeiro, Luiz A. S.. "Phenolic Lipids Derived from Cashew Nut Shell Liquid to Treat Metabolic Diseases". . p. 1961 - 1978. Retrieved 2022/02/14.
• 2、 Sridhar, Uma,Pramod,Jayakannan. "Creation of dextrin vesicles and their loading-delivering capabilities". . p. 21237 - 21241. Retrieved 2013/11/06.